Co(ClC₆H₄NC)2(P(OC₂H₅)2C₆H₅)3⁽¹⁺⁾*PF₆^(1-)=Co(ClC₆H₄NC)2(P(OC₂H₅)2C₆H₅)3PF₆

Base Information

• Chemical Name: Co(ClC₆H₄NC)2(P(OC₂H₅)2C₆H₅)3⁽¹⁺⁾*PF₆^(1-)=Co(ClC₆H₄NC)2(P(OC₂H₅)2C₆H₅)3PF₆
• CAS No.: 131612-02-7
• Molecular Formula: C₄₄H₅₃Cl₂CoN₂O₆P₃*F₆P
• Molecular Weight: 1073.7

Synonyms:

Chemical Property of Co(ClC₆H₄NC)2(P(OC₂H₅)2C₆H₅)3⁽¹⁺⁾*PF₆^(1-)=Co(ClC₆H₄NC)2(P(OC₂H₅)2C₆H₅)3PF₆

Chemical Property:

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Technology Process of Co(ClC₆H₄NC)2(P(OC₂H₅)2C₆H₅)3⁽¹⁺⁾*PF₆^(1-)=Co(ClC₆H₄NC)2(P(OC₂H₅)2C₆H₅)3PF₆

There total 2 articles about Co(ClC₆H₄NC)2(P(OC₂H₅)2C₆H₅)3⁽¹⁺⁾*PF₆^(1-)=Co(ClC₆H₄NC)2(P(OC₂H₅)2C₆H₅)3PF₆ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 70.0%

CoH(P(OC2H5)2(C6H5))4(1+)*ClO4(1-)=CoH(P(OC2H5)2(C6H5))4ClO4 (131611-98-8) + p-chlorophenyl isocyanide (1885-81-0) → Co(ClC6H4NC)2(P(OC2H5)2C6H5)3(1+)*PF6(1-)=Co(ClC6H4NC)2(P(OC2H5)2C6H5)3PF6 (131612-02-7)

Guidance literature:

With NaPF₆; In ethanol; dichloromethane; addn. of an excess of isocyanide to soln. of Co-compd. (under Ar, Schlenk app.) in CH2Cl2, cooling to -80°C, then warming to room temp., stirring for 20 min; solvent removal under reduced pressure, treating of residue with EtOH, then addn. of NaPF6 in EtOH, crystn. by slow cooling of its saturated soln. in EtOH at about 30-40°C, elem. anal.;

DOI:10.1039/DT9900002979

Reference yield:

CoH2(P(OC2H5)2C6H5)4(1+)*B(C6H5)4(1-)=CoH2(P(OC2H5)2C6H5)4B(C6H5)4 + p-chlorophenyl isocyanide (1885-81-0) → Co(ClC6H4NC)2(P(OC2H5)2C6H5)3(1+)*PF6(1-)=Co(ClC6H4NC)2(P(OC2H5)2C6H5)3PF6 (131612-02-7)

Guidance literature:

With NaPF₆; In not given; react. of Co-compd with isocyanide, addn. of NaPF6;

DOI:10.1039/DT9900002979

Reference yield:

Co(CNC6H4Cl)2(P(C6H5)(OC2H5)2)3(1+)*PF6(1-)={Co(CNC6H4Cl)2(C6H5P(OC2H5)2)3}PF6 (131612-02-7) + 4-methylbenzenediazonium tetrafluoroborate (459-44-9) + 1,2-dichloro-ethane (107-06-2,52399-93-6) → {Co(ClCHCH2Cl)(CNC6H4Cl)2(C6H5P(OC2H5)2)3}(2+)

Guidance literature:

In 1,2-dichloro-ethane; byproducts: nitrogen, toluene; inert atmosphere;

DOI:10.1021/om00158a001

upstream raw materials:

CoH(P(OC₂H₅)2(C₆H₅))4⁽¹⁺⁾*ClO₄^(1-)=CoH(P(OC₂H₅)2(C₆H₅))4ClO₄

p-chlorophenyl isocyanide

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