-4-(1-methylethyl)-3-(2-methyl-1-oxo-3-phenyl-2-propenyl)-2-oxazolidinone

Base Information

Chemical Name:-4-(1-methylethyl)-3-(2-methyl-1-oxo-3-phenyl-2-propenyl)-2-oxazolidinone
CAS No.:136057-73-3
Molecular Formula:C₁₆H₁₉NO₃
Molecular Weight:273.332
Hs Code.:

<S-(E)>-4-(1-methylethyl)-3-(2-methyl-1-oxo-3-phenyl-2-propenyl)-2-oxazolidinone

Synonyms:

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of -4-(1-methylethyl)-3-(2-methyl-1-oxo-3-phenyl-2-propenyl)-2-oxazolidinone

Chemical Property:

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Technology Process of -4-(1-methylethyl)-3-(2-methyl-1-oxo-3-phenyl-2-propenyl)-2-oxazolidinone

There total 1 articles about -4-(1-methylethyl)-3-(2-methyl-1-oxo-3-phenyl-2-propenyl)-2-oxazolidinone which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 35086-87-4,38449-13-7
(E)-2-methyl-3-phenylacryloyl chloride

: 17016-83-0
(4S)-4-isopropyl-1,3-oxazolidin-2-one

: 136057-73-3
-4-(1-methylethyl)-3-(2-methyl-1-oxo-3-phenyl-2-propenyl)-2-oxazolidinone

Guidance literature:: With n-butyllithium; Multistep reaction; 1) THF, hexane, -78 deg C;
DOI:10.1016/S0040-4020(96)01191-X

Reference yield:

: 136057-73-3
-4-(1-methylethyl)-3-(2-methyl-1-oxo-3-phenyl-2-propenyl)-2-oxazolidinone

: 108-98-5
thiophenol

: 136088-23-8
(S)-4-Isopropyl-3-((2S,3S)-2-methyl-3-phenyl-3-phenylsulfanyl-propionyl)-oxazolidin-2-one

: 136088-24-9
(S)-4-Isopropyl-3-((2S,3R)-2-methyl-3-phenyl-3-phenylsulfanyl-propionyl)-oxazolidin-2-one

: 136057-79-9
(S)-4-Isopropyl-3-((2R,3S)-2-methyl-3-phenyl-3-phenylsulfanyl-propionyl)-oxazolidin-2-one

: 136088-22-7
(S)-4-Isopropyl-3-((2R,3R)-2-methyl-3-phenyl-3-phenylsulfanyl-propionyl)-oxazolidin-2-one

Guidance literature:: With lithium thiophenoxide; In tetrahydrofuran; at 0 ℃; Yield given. Yields of byproduct given;
DOI:10.1016/0040-4039(91)80821-M

Reference yield:

: 136057-73-3
-4-(1-methylethyl)-3-(2-methyl-1-oxo-3-phenyl-2-propenyl)-2-oxazolidinone

: 79563-27-2
4(S)-(1-methylethyl)-3-(2(R)-methyl-1-oxo-3-phenylpropyl)-2-oxazolidinone

Guidance literature:: Multi-step reaction with 2 steps

1: 1.) n-BuLi / 1) THF, hexane, 0 deg C; 2) THF, hexane, 0 deg C, 5 h

2: 90 percent / Raney-Ni / ethanol / Heating

With n-butyllithium; nickel; In ethanol;
DOI:10.1016/S0040-4020(96)01191-X