Dichlorobis[2-(di-t-butylphosphino)ethylamine]ruthenium(II),min.97%

Base Information

• Chemical Name: Dichlorobis[2-(di-t-butylphosphino)ethylamine]ruthenium(II),min.97%
• CAS No.: 1092372-91-2
• Molecular Formula: C20H48Cl2N2P2Ru
• Molecular Weight: 550.532042
• Hs Code.: 28439090
• Mol file: 1092372-91-2.mol

Synonyms:Dichlorobis[2-(di-t-butylphosphino)ethylamine]ruthenium(II),min.97%;Dichlorobis[2-(di-t-butylphosphino)ethylaMine]rutheniuM(II),97%

Chemical Property of Dichlorobis[2-(di-t-butylphosphino)ethylamine]ruthenium(II),min.97%

Chemical Property:

• PSA: 79.22000
• LogP: 1.45660

Purity/Quality:

98%,99%, ^*data from raw suppliers

Dichlorobis[2-(di-t-butylphosphino)ethylamine]ruthenium(II), min. 97% ^*data from reagent suppliers

Safty Information:

• Pictogram(s):  
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MSDS Files:

SDS file from LookChem

Useful:

Technology Process of Dichlorobis[2-(di-t-butylphosphino)ethylamine]ruthenium(II),min.97%

There total 3 articles about Dichlorobis[2-(di-t-butylphosphino)ethylamine]ruthenium(II),min.97% which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 88.0%

cyclooctadiene ruthenium(II) dichloride (50982-12-2) + 2-(di-tert-butylphosphino)ethylamine (1053658-84-6) → trans-RuCl2((t-Bu)2P(CH2)2NH2)2 (1092372-91-2)

Guidance literature:

In toluene; a mixt. of complex and aminophosphine was refluxed in toluene under Ar for 8 h, the mixt. was cooled to room temp.; ether was added, suspn. was stirred for 1 h, filtered, washed with etherand dried under vac.; elem. anal.;

DOI:10.1039/b911459a

Reference yield:

2-(di-tert-butylphosphino)ethylamine (1053658-84-6) → RuCl2(tBu2PCH2CH2NH2)2 (1092372-91-2)

Guidance literature:

In toluene; for 6h; Inert atmosphere; Schlenk technique; Glovebox; Reflux;

Reference yield:

cyclooctadiene ruthenium(II) dichloride (50982-12-2) + 2-(di-tert-butylphosphino)ethylamine (1053658-84-6) → trans-RuCl2((t-Bu)2P(CH2)2NH2)2 (1092372-91-2) + cis-RuCl2((t-Bu)2P(CH2)2NH2)2

Guidance literature:

In tetrahydrofuran; a mixt. of complex and aminophosphine was refluxed in THF under Ar for 6h, the mixt. was cooled to room temp.; the mixt. of isomers;

DOI:10.1039/b911459a

upstream raw materials:

cyclooctadiene ruthenium(II) dichloride

2-(di-tert-butylphosphino)ethylamine

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