2-(Di-t-butylphosphino)ethylamine, min. 97% (10 wt% in THF)

Base Information

Chemical Name:2-(Di-t-butylphosphino)ethylamine, min. 97% (10 wt% in THF)
CAS No.:1053658-84-6
Molecular Formula:C10H24NP
Molecular Weight:189.278021
Hs Code.:2931900090
Mol file:1053658-84-6.mol

Synonyms:2-(Di-t-butylphosphino)ethylamine, min. 97% (10 wt% in THF);2-(Di-t-butylphosphino)ethylaMine;2-(Di-tert-butylphosphino)ethylaMine, 10 wt.% solution in THF;2-(Di-tert-butylphosphino)ethylaMine, 10% w/w soln. in THF;2-(Di-tert-butylphosphino)ethylamine solution

Suppliers and Price of 2-(Di-t-butylphosphino)ethylamine, min. 97% (10 wt% in THF)

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Strem Chemicals
2-(Di-t-butylphosphino)ethylamine, min. 97% (10 wt% in THF)
25g
$ 314.00

Strem Chemicals
2-(Di-t-butylphosphino)ethylamine, min. 97% (10 wt% in THF)
5g
$ 79.00

Sigma-Aldrich
2-(Di-tert-butylphosphino)ethylamine 10wt. % in THF
25g
$ 347.00

Sigma-Aldrich
2-(Di-tert-butylphosphino)ethylamine 10wt. % in THF
5g
$ 84.10

American Custom Chemicals Corporation
2-(DI-TERT-BUTYLPHOSPHINO)ETHYLAMINE 95.00%
5MG
$ 503.47

Total 11 raw suppliers

Chemical Property of 2-(Di-t-butylphosphino)ethylamine, min. 97% (10 wt% in THF)

Chemical Property:

Refractive Index:n20/D1.420
Boiling Point:238.7±23.0 °C(Predicted)
PKA:10.13±0.10(Predicted)
Flash Point:-20℃
PSA：39.61000
Density:0.879 g/mL at 25 °C
LogP:3.72430
Sensitive.:air sensitive, moisture sensitiv

Purity/Quality:

97% ^*data from raw suppliers

2-(Di-t-butylphosphino)ethylamine, min. 97% (10 wt% in THF) ^*data from reagent suppliers

Safty Information:

Pictogram(s):
Hazard Codes:F+,C,F
Statements: 17-34-40-37-19-11
Safety Statements: 26-36/37/39-45-16

MSDS Files:: SDS file from LookChem

Useful:

Technology Process of 2-(Di-t-butylphosphino)ethylamine, min. 97% (10 wt% in THF)

There total 3 articles about 2-(Di-t-butylphosphino)ethylamine, min. 97% (10 wt% in THF) which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 61.0%

: 819-19-2
di-tert-butylphosphine

: 61883-48-5
N, N′-bis(trimethylsilyl)-2-chloroethanamine

: 1053658-84-6
2-(di-tert-butylphosphino)ethylamine

Guidance literature:: di-tert-butylphosphine; With n-butyllithium; In hexane; at -78 - 20 ℃; Schlenk technique;

N, N′-bis(trimethylsilyl)-2-chloroethanamine; In hexane; at 20 - 80 ℃; for 8.5h; Further stages;
DOI:10.1021/jacs.6b04271

Reference yield:

: 13716-10-4
di(tert-butyl)chlorophosphine

: 61883-48-5
N, N′-bis(trimethylsilyl)-2-chloroethanamine

: 1053658-84-6
2-(di-tert-butylphosphino)ethylamine

Guidance literature:: di(tert-butyl)chlorophosphine; With lithium; In tetrahydrofuran; at 0 - 20 ℃; for 72h;

N, N′-bis(trimethylsilyl)-2-chloroethanamine; In tetrahydrofuran; at 0 ℃; for 4h; Heating / reflux;

With sodium hydroxide; sulfuric acid; water; more than 3 stages;

Reference yield:

: C₁₆H₄₀NPSi₂

: 1053658-84-6
2-(di-tert-butylphosphino)ethylamine

Guidance literature:: C₁₆H₄₀NPSi₂; With sulfuric acid; water; In tetrahydrofuran; at 20 ℃; for 1h;

With sodium hydroxide; In tetrahydrofuran; water; for 1h;
DOI:10.1039/b911459a