C₅₅H₅₇Cl₂N₅O₁₇

Base Information

• Chemical Name: C₅₅H₅₇Cl₂N₅O₁₇
• CAS No.: 145007-47-2
• Molecular Formula: C₅₅H₅₇Cl₂N₅O₁₇
• Molecular Weight: 1130.99
• Mol file: 145007-47-2.mol

Synonyms:

Chemical Property of C₅₅H₅₇Cl₂N₅O₁₇

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of C₅₅H₅₇Cl₂N₅O₁₇

There total 4 articles about C₅₅H₅₇Cl₂N₅O₁₇ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

di-tert-butyl dicarbonate (24424-99-5) → C55H57Cl2N5O17 (145007-47-2)

Guidance literature:

Multi-step reaction with 2 steps

1: 100 percent / NaHCO₃ / dioxane; H₂O / 5 h / Ambient temperature

2: 6.4 g / TsOH / acetone / 1.5 h / Ambient temperature

With sodium hydrogencarbonate; toluene-4-sulfonic acid; In 1,4-dioxane; water; acetone;

DOI:10.1021/jo9506746

Reference yield:

C58H49Cl2N7O18 → C55H57Cl2N5O17 (145007-47-2)

Guidance literature:

Multi-step reaction with 3 steps

1: 1.) PhNCS, 2.) CF₃CO₂H / 1.) Py, H₂O, room temperature, 7 h, 2.) room temperature, 1.5 h

2: 100 percent / NaHCO₃ / dioxane; H₂O / 5 h / Ambient temperature

3: 6.4 g / TsOH / acetone / 1.5 h / Ambient temperature

With sodium hydrogencarbonate; phenyl isothiocyanate; toluene-4-sulfonic acid; trifluoroacetic acid; In 1,4-dioxane; water; acetone;

DOI:10.1021/jo9506746

Reference yield:

C42H37Cl2N5O13 (145007-45-0) → C55H57Cl2N5O17 (145007-47-2)

Guidance literature:

Multi-step reaction with 2 steps

1: 100 percent / NaHCO₃ / dioxane; H₂O / 5 h / Ambient temperature

2: 6.4 g / TsOH / acetone / 1.5 h / Ambient temperature

With sodium hydrogencarbonate; toluene-4-sulfonic acid; In 1,4-dioxane; water; acetone;

DOI:10.1021/jo9506746

upstream raw materials:

2,2-dimethoxy-propane

C₅₂H₅₃Cl₂N₅O₁₇

di-tert-butyl dicarbonate

C₄₂H₃₇Cl₂N₅O₁₃