hydrido(3-diphenylphosphino)thiophenolato-[P,S]-bis(trimethylphosphine)nickel(II)

Base Information

Chemical Name:hydrido(3-diphenylphosphino)thiophenolato-[P,S]-bis(trimethylphosphine)nickel(II)
CAS No.:926319-61-1
Molecular Formula:C₂₄H₃₃NiP₃S
Molecular Weight:505.203
Hs Code.:

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Chemical Property of hydrido(3-diphenylphosphino)thiophenolato-[P,S]-bis(trimethylphosphine)nickel(II)

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Technology Process of hydrido(3-diphenylphosphino)thiophenolato-[P,S]-bis(trimethylphosphine)nickel(II)

There total 4 articles about hydrido(3-diphenylphosphino)thiophenolato-[P,S]-bis(trimethylphosphine)nickel(II) which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 37.0%

: 28069-69-4
tetrakis(trimethylphosphine)nickel⁽⁰⁾

: 119327-17-2
(2-mercaptophenyl)diphenylphosphine

: 926319-61-1
hydrido(3-diphenylphosphino)thiophenolato-[P,S]-bis(trimethylphosphine)nickel(II)

Guidance literature:: With trimethylphosphine; In pentane; to soln. Ni(PMe3)4 in pentane 2-diphenylphosphinothiophenol and PMe3 were added and stirred at room temp. for 16 h; soln. was filtered and kept at -27°C; elem. anal.;
DOI:10.1021/om0606340

Reference yield: 37.0%

: 28069-69-4
tetrakis(trimethylphosphine)nickel⁽⁰⁾

: 119327-17-2
(2-mercaptophenyl)diphenylphosphine

: 594-09-2
trimethylphosphane

: 926319-61-1
hydrido(2-diphenylphosphanyl)thiophenolato[P,S]bis(trimethylphosphine)nickel

Guidance literature:: In pentane; byproducts: trimetylphosphine; combining of soln. of Ni(PMe3)4 in pentane containing excess trimethylphosphine with (2-diphenylphosphanyl)thiophenol; stirring for 30 min; filtration, cooling to -27°C; crystn., elem. anal.;
DOI:10.1016/j.jorganchem.2009.01.023

Reference yield: 30.0%

: 101077-61-6
(cyclooctadiene)bis(trimethylphosphino)nickel

: 119327-17-2
(2-mercaptophenyl)diphenylphosphine

: 594-09-2
trimethylphosphane

: 926319-61-1
hydrido(2-diphenylphosphanyl)thiophenolato[P,S]bis(trimethylphosphine)nickel

Guidance literature:: In not given; combining of Ni(1,5-cyclooctadiene)(PMe3)2 with (2-diphenylphosphanyl)thiophenol in the presence of excess PMe3;
DOI:10.1016/j.jorganchem.2009.01.023