1.1.8.8-tetraphenyl-1.8-distanna cycloetraceca-2.6.9.13-tetraene

Base Information

• Chemical Name: 1.1.8.8-tetraphenyl-1.8-distanna cycloetraceca-2.6.9.13-tetraene
• CAS No.: 24959-44-2
• Molecular Formula: C₃₆H₃₆Sn₂
• Molecular Weight: 706.102
• Mol file: 24959-44-2.mol

Synonyms:

Chemical Property of 1.1.8.8-tetraphenyl-1.8-distanna cycloetraceca-2.6.9.13-tetraene

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of 1.1.8.8-tetraphenyl-1.8-distanna cycloetraceca-2.6.9.13-tetraene

There total 3 articles about 1.1.8.8-tetraphenyl-1.8-distanna cycloetraceca-2.6.9.13-tetraene which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 34.0%

1,1-diphenyl-4,5-dihydro-1H-stannepine (24959-43-1,28483-45-6) → 1.1.8.8-tetraphenyl-1.8-distanna cycloetraceca-2.6.9.13-tetraene (24959-44-2)

Guidance literature:

In diethyl ether; Irradiation (UV/VIS); irradiation for 1h;;

DOI:10.1016/S0040-4039(01)88381-7

Reference yield:

→ 1,1,8,8-Tetraphenyl-1,8-distanna-cyclotetradeca-2,6,9,13-tetraen (24959-44-2)

Guidance literature:

aus 1,1-Diphenyl-1-stanna-cyclohepta-2,6-dien u. hν;

DOI:10.1016/S0040-4039(01)88381-7

Reference yield:

diphenyltin (1011-95-6) + hexa-1,5-diyne (628-16-0) → 1.1.8.8-tetraphenyl-1.8-distanna cycloetraceca-2.6.9.13-tetraene (24959-44-2)

Guidance literature:

Multi-step reaction with 2 steps

1: hexane

2: diethyl ether

In diethyl ether; hexane;

upstream raw materials:

1,1-diphenyl-4,5-dihydro-1H-stannepine

diphenyltin

hexa-1,5-diyne