HRu₄(CO)12BHAu(P(CH₃C₆H₄)3)

Base Information

Chemical Name:HRu₄(CO)12BHAu(P(CH₃C₆H₄)3)
CAS No.:141292-27-5
Molecular Formula:C₃₃H₂₃AuBO₁₂PRu₄
Molecular Weight:1254.57
Hs Code.:

HRu<sub>4</sub>(CO)12BHAu(P(CH<sub>3</sub>C<sub>6</sub>H<sub>4</sub>)3)

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Chemical Property of HRu₄(CO)12BHAu(P(CH₃C₆H₄)3)

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Technology Process of HRu₄(CO)12BHAu(P(CH₃C₆H₄)3)

There total 1 articles about HRu₄(CO)12BHAu(P(CH₃C₆H₄)3) which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 15.0%

: {bis(triphenylphosphine)nitrogen}{HRu₄(CO)12BH}

: 28978-10-1
chloro{tris(o-tolyl)phosphine}gold(I)

: 141292-34-4
Ru₄(CO)12BHAu₂(P(CH₃C₆H₄)3)2

: 141319-39-3
Ru₄(CO)12BHAu₂(P(CH₃C₆H₄)3)2

: 141292-27-5
HRu₄(CO)12BHAu(P(CH₃C₆H₄)3)

: 141292-29-7
Ru₄BAu₃*12CO*3P(CH₃C₆H₄)3=Ru₄(CO)12BAu₃(P(CH₃C₆H₄)3)3

Guidance literature:: With TlPF₆; In dichloromethane; byproducts: H4Ru4(CO)12; react. under Ar (Schlenk technique); addn. of CH2Cl2 to a mixture of Ru-complex, Au-compd. and TlPF6, stirring for 15 min (color change from orange to dark brown); sepn. by TLC (Kieselgel), elution with CH2Cl2-hexane (1:1), 1. band is H4Ru(CO)12; 2. (yellow) is Au(P(2-MeC6H4)3)2((HRu4(CO)12BH)2Au); 3. (dark orange) is monogold-compd., 4. (bright orange) is digold-compd. (2 isomers, detd. by NMR), trigold-compd.;

Reference yield:

: 141292-27-5
HRu₄(CO)12BHAu(P(CH₃C₆H₄)3)

: 141319-36-0
(CH₃CH₂)3NH⁽¹⁺⁾*HRu₄(CO)12BAu(P(CH₃C₆H₄)3)^(1-)=((CH₃CH₂)3NH)(HRu₄(CO)12BAu(P(CH₃C₆H₄)3))

Guidance literature:: With (C₂H₅)3N; In dichloromethane; react. under Ar (Schlenk technique); addn. of Et3N to Ru-complex in CH2Cl2 (color change from red-orange to dark-brown); evapn., washing with hexane;