3-m-nitrobenzoyl butyric acid

Base Information

Chemical Name:3-m-nitrobenzoyl butyric acid
CAS No.:42075-28-5
Molecular Formula:C₁₁H₁₁NO₅
Molecular Weight:237.212
Hs Code.:

Synonyms:

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 3-m-nitrobenzoyl butyric acid

Chemical Property:

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Technology Process of 3-m-nitrobenzoyl butyric acid

There total 4 articles about 3-m-nitrobenzoyl butyric acid which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 17408-16-1
3'-nitropropiophenone

: 42075-28-5
3-m-nitrobenzoyl butyric acid

Guidance literature:: Multi-step reaction with 3 steps

1.1: 89 percent / Br₂ / acetic acid

2.1: NaH / dimethylformamide / 20 °C

2.2: dimethylformamide / 4 h / 110 °C

3.1: aq. HCl / 6 h / Heating

With hydrogenchloride; bromine; sodium hydride; In acetic acid; N,N-dimethyl-formamide;
DOI:10.1021/jm030776l

Reference yield:

: 1205-36-3
2-bromo-1-(3-nitrophenyl)propan-1-one

: 42075-28-5
3-m-nitrobenzoyl butyric acid

Guidance literature:: Multi-step reaction with 2 steps

1.1: NaH / dimethylformamide / 20 °C

1.2: dimethylformamide / 4 h / 110 °C

2.1: aq. HCl / 6 h / Heating

With hydrogenchloride; sodium hydride; In N,N-dimethyl-formamide;
DOI:10.1021/jm030776l