C₁₅H₁₂ClN₃

Base Information

• Chemical Name: C₁₅H₁₂ClN₃
• CAS No.: 79158-56-8
• Molecular Formula: C₁₅H₁₂ClN₃
• Molecular Weight: 269.733
• Mol file: 79158-56-8.mol

Synonyms:

Chemical Property of C₁₅H₁₂ClN₃

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of C₁₅H₁₂ClN₃

There total 6 articles about C₁₅H₁₂ClN₃ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

1,2-diphenylprop-2-en-1-one (4452-11-3) → C15H12ClN3 (79158-56-8)

Guidance literature:

Multi-step reaction with 2 steps

1: phosphorus pentachloride / CH₂Cl₂ / 48 h / Heating

2: N₃^(1-)

With phosphorus pentachloride; azide^(1-); In dichloromethane;

DOI:10.1016/S0040-4039(01)81784-6

Reference yield:

(1-chloroethene-1,2-diyl)dibenzene (1460-06-6) → C15H12ClN3 (79158-56-8)

Guidance literature:

Multi-step reaction with 3 steps

1: chlorine azide, base

3: diethyl ether / 3 h / 0 °C

With chlorine azide; In diethyl ether;

DOI:10.1016/S0040-4039(01)81784-6

Reference yield:

diazomethane (186581-53-3,908094-01-9,334-88-3) + diphenylchloroazirine (72040-08-5) → C15H12ClN3 + C15H12ClN3 (79158-56-8)

Guidance literature:

In diethyl ether; at 0 ℃; for 3h;

DOI:10.1016/S0040-4039(01)81784-6

upstream raw materials:

diazomethane

diphenylchloroazirine

C₁₅H₁₂Cl₂

1,2-diphenylprop-2-en-1-one

Downstream raw materials:

2-Chloromethyl-2,3-diphenyl-2H-azirine

Refernces