Bis<1-(4-chlorphenyl)-2,2-dimethylpropyl>diazen

Base Information

• Chemical Name: Bis<1-(4-chlorphenyl)-2,2-dimethylpropyl>diazen
• CAS No.: 68525-44-0
• Molecular Formula: C₂₂H₂₈Cl₂N₂
• Molecular Weight: 391.384
• Mol file: 68525-44-0.mol

Synonyms:

Chemical Property of Bis<1-(4-chlorphenyl)-2,2-dimethylpropyl>diazen

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of Bis<1-(4-chlorphenyl)-2,2-dimethylpropyl>diazen

There total 3 articles about Bis<1-(4-chlorphenyl)-2,2-dimethylpropyl>diazen which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 66.0%

1,2-Bis<1-(4-chlorphenyl)-2,2-dimethylpropyl>hydrazin (86439-94-3) → Bis<1-(4-chlorphenyl)-2,2-dimethylpropyl>diazen (68525-44-0)

Guidance literature:

With mercury(II) oxide; In diethyl ether; for 50h; Heating;

Reference yield:

1-(4-chlorophenyl)-2,2-dimethylpropan-1-one (30314-42-2) → Bis<1-(4-chlorphenyl)-2,2-dimethylpropyl>diazen (68525-44-0)

Guidance literature:

Multi-step reaction with 3 steps

1: 82 percent / 100percent hydrazine hydrate / ethanol; acetic acid / Heating

2: 52 percent / H₂ / Pd/C (10percent) / cyclohexane / 24 h / 25 °C / 36775.4 Torr

3: 66 percent / HgO / diethyl ether / 50 h / Heating

With hydrogen; hydrazine hydrate; mercury(II) oxide; palladium on activated charcoal; In diethyl ether; ethanol; cyclohexane; acetic acid;

Reference yield:

4-Chlorpivalophenonazin (54953-06-9) → Bis<1-(4-chlorphenyl)-2,2-dimethylpropyl>diazen (68525-44-0)

Guidance literature:

Multi-step reaction with 2 steps

1: 52 percent / H₂ / Pd/C (10percent) / cyclohexane / 24 h / 25 °C / 36775.4 Torr

2: 66 percent / HgO / diethyl ether / 50 h / Heating

With hydrogen; mercury(II) oxide; palladium on activated charcoal; In diethyl ether; cyclohexane;

upstream raw materials:

1,2-Bis<1-(4-chlorphenyl)-2,2-dimethylpropyl>hydrazin

1-(4-chlorophenyl)-2,2-dimethylpropan-1-one

4-Chlorpivalophenonazin

Downstream raw materials:

meso-3,4-Bis(4-chlorphenyl)-2,2,5,5-tetramethylhexan

DL-3,4-Bis(4-chlorphenyl)-2,2,5,5-tetramethylhexan

Refernces