N'-{2-cyano-9-[(4-methyl-1-piperazinyl)carbonyl]-9H-purin-6-yl}-N'-cyclohexyl-4-[(4-methyl-1-piperazinyl)methyl]benzohydrazide trifluoroacetate

Base Information

Chemical Name:N'-{2-cyano-9-[(4-methyl-1-piperazinyl)carbonyl]-9H-purin-6-yl}-N'-cyclohexyl-4-[(4-methyl-1-piperazinyl)methyl]benzohydrazide trifluoroacetate
CAS No.:1055925-82-0
Molecular Formula:C₂HF₃O₂*C₃₁H₄₁N₁₁O₂
Molecular Weight:713.763
Hs Code.:

N'-{2-cyano-9-[(4-methyl-1-piperazinyl)carbonyl]-9H-purin-6-yl}-N'-cyclohexyl-4-[(4-methyl-1-piperazinyl)methyl]benzohydrazide trifluoroacetate

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Chemical Property of N'-{2-cyano-9-[(4-methyl-1-piperazinyl)carbonyl]-9H-purin-6-yl}-N'-cyclohexyl-4-[(4-methyl-1-piperazinyl)methyl]benzohydrazide trifluoroacetate

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Technology Process of N'-{2-cyano-9-[(4-methyl-1-piperazinyl)carbonyl]-9H-purin-6-yl}-N'-cyclohexyl-4-[(4-methyl-1-piperazinyl)methyl]benzohydrazide trifluoroacetate

There total 5 articles about N'-{2-cyano-9-[(4-methyl-1-piperazinyl)carbonyl]-9H-purin-6-yl}-N'-cyclohexyl-4-[(4-methyl-1-piperazinyl)methyl]benzohydrazide trifluoroacetate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 1055925-81-9
N'-{2-cyano-9-[(4-methyl-1-piperazinyl)carbonyl]-9H-purin-6-yl}-N'-cyclohexyl-4-[(4-methyl-1-piperazinyl)methyl]benzohydrazide

: 76-05-1
trifluoroacetic acid

: 1055925-82-0
N'-{2-cyano-9-[(4-methyl-1-piperazinyl)carbonyl]-9H-purin-6-yl}-N'-cyclohexyl-4-[(4-methyl-1-piperazinyl)methyl]benzohydrazide trifluoroacetate

Guidance literature:: In water; acetonitrile;

Reference yield:

: 1055927-38-2
6-(1-cyclohexylhydrazino)-9-[(4-methyl-1-piperazinyl)carbonyl]-9H-purine-2-carbonitrile

: 1055925-82-0
N'-{2-cyano-9-[(4-methyl-1-piperazinyl)carbonyl]-9H-purin-6-yl}-N'-cyclohexyl-4-[(4-methyl-1-piperazinyl)methyl]benzohydrazide trifluoroacetate

Guidance literature:: Multi-step reaction with 3 steps

1: N-ethyl-N,N-diisopropylamine / tetrahydrofuran / 0 °C

2: N-ethyl-N,N-diisopropylamine / tetrahydrofuran / 3 h / 20 °C

3: water; acetonitrile

With N-ethyl-N,N-diisopropylamine; In tetrahydrofuran; water; acetonitrile;

Reference yield:

: 1055925-71-7
1,1-dimethylethyl 2-{2-cyano-9-[(4-methyl-1-piperazinyl)carbonyl]-9H-purin-6-yl}-2-cyclohexylhydrazinecarboxylate

: 1055925-82-0
N'-{2-cyano-9-[(4-methyl-1-piperazinyl)carbonyl]-9H-purin-6-yl}-N'-cyclohexyl-4-[(4-methyl-1-piperazinyl)methyl]benzohydrazide trifluoroacetate

Guidance literature:: Multi-step reaction with 5 steps

1: water; acetonitrile

2: toluene-4-sulfonic acid / water; acetonitrile / 20 °C

3: N-ethyl-N,N-diisopropylamine / tetrahydrofuran / 0 °C

4: N-ethyl-N,N-diisopropylamine / tetrahydrofuran / 3 h / 20 °C

5: water; acetonitrile

With toluene-4-sulfonic acid; N-ethyl-N,N-diisopropylamine; In tetrahydrofuran; water; acetonitrile;