2-(2-cyanoethyl)-3-(p-methoxyphenyl)-4-cyanoisoxazolidine

Base Information

• Chemical Name: 2-(2-cyanoethyl)-3-(p-methoxyphenyl)-4-cyanoisoxazolidine
• CAS No.: 89902-79-4
• Molecular Formula: C₁₄H₁₅N₃O₂
• Molecular Weight: 257.292
• Mol file: 89902-79-4.mol

Synonyms:

Chemical Property of 2-(2-cyanoethyl)-3-(p-methoxyphenyl)-4-cyanoisoxazolidine

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of 2-(2-cyanoethyl)-3-(p-methoxyphenyl)-4-cyanoisoxazolidine

There total 3 articles about 2-(2-cyanoethyl)-3-(p-methoxyphenyl)-4-cyanoisoxazolidine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

p-methoxyl benzaldoxime (3717-21-3,3717-22-4,140461-28-5,140461-29-6,3235-04-9) + acrylonitrile (107-13-1,25014-41-9) → 2-(2-cyanoethyl)-3-(p-methoxyphenyl)-4-cyanoisoxazolidine (89902-78-3,89902-79-4) + 2-(2-cyanoethyl)-3-(p-methoxyphenyl)-5-cyanoisoxazolidine

Guidance literature:

With hydroquinone; at 120 ℃; for 18h;

DOI:10.1080/00397919408012640

Reference yield:

p-methoxyl benzaldoxime (3717-21-3,3717-22-4,140461-28-5,140461-29-6,3235-04-9) + acrylonitrile (107-13-1,25014-41-9) → 2-(2-cyanoethyl)-3-(p-methoxyphenyl)-5-cyanoisoxazolidine (89902-76-1,89902-77-2) + 2-(2-cyanoethyl)-3-(p-methoxyphenyl)-5-cyanoisoxazolidine (89902-76-1,89902-77-2) + 2-(2-cyanoethyl)-3-(p-methoxyphenyl)-4-cyanoisoxazolidine (89902-78-3,89902-79-4) + 2-(2-cyanoethyl)-3-(p-methoxyphenyl)-4-cyanoisoxazolidine (89902-78-3,89902-79-4)

Guidance literature:

In pyridine; at 80 - 85 ℃; Yield given. Yields of byproduct given;

DOI:10.1039/P19840000047

Reference yield:

p-methoxyl benzaldoxime (3717-21-3,3717-22-4,140461-28-5,140461-29-6,3235-04-9) + acrylonitrile (107-13-1,25014-41-9) → 2-(2-cyanoethyl)-3-(p-methoxyphenyl)-5-cyanoisoxazolidine (89902-76-1,89902-77-2) + 2-(2-cyanoethyl)-3-(p-methoxyphenyl)-5-cyanoisoxazolidine (89902-76-1,89902-77-2) + 2-(2-cyanoethyl)-3-(p-methoxyphenyl)-4-cyanoisoxazolidine (89902-78-3,89902-79-4) + 2-(2-cyanoethyl)-3-(p-methoxyphenyl)-4-cyanoisoxazolidine (89902-78-3,89902-79-4)

Guidance literature:

In pyridine; at 80 - 85 ℃; Yield given. Yields of byproduct given;

DOI:10.1039/P19840000047

upstream raw materials:

p-methoxyl benzaldoxime

acrylonitrile