Technology Process of C23H23F13O6
There total 5 articles about C23H23F13O6 which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
Multi-step reaction with 4 steps
1: 100 percent / H2 / Pd/C / ethyl acetate / 20 °C
2: 95 percent / red-Al; pyrrolidine; t-BuOK / tetrahydrofuran / -20 - 0 °C
3: p-TsOH*H2O; Na2SO4 / acetonitrile / 20 °C
4: acetonitrile
With
pyrrolidine; potassium tert-butylate; hydrogen; toluene-4-sulfonic acid; sodium sulfate; sodium bis(2-methoxyethoxy)aluminium dihydride;
palladium on activated charcoal;
In
tetrahydrofuran; ethyl acetate; acetonitrile;
DOI:10.1016/j.tetlet.2007.04.106
- Guidance literature:
-
Multi-step reaction with 5 steps
1: 100 percent / K2CO3 / dioxane; H2O / Heating
2: 100 percent / H2 / Pd/C / ethyl acetate / 20 °C
3: 95 percent / red-Al; pyrrolidine; t-BuOK / tetrahydrofuran / -20 - 0 °C
4: p-TsOH*H2O; Na2SO4 / acetonitrile / 20 °C
5: acetonitrile
With
pyrrolidine; potassium tert-butylate; hydrogen; potassium carbonate; toluene-4-sulfonic acid; sodium sulfate; sodium bis(2-methoxyethoxy)aluminium dihydride;
palladium on activated charcoal;
In
tetrahydrofuran; 1,4-dioxane; water; ethyl acetate; acetonitrile;
1: Wittig reaction;
DOI:10.1016/j.tetlet.2007.04.106
- Guidance literature:
-
Multi-step reaction with 2 steps
1: p-TsOH*H2O; Na2SO4 / acetonitrile / 20 °C
2: acetonitrile
With
toluene-4-sulfonic acid; sodium sulfate;
In
acetonitrile;
DOI:10.1016/j.tetlet.2007.04.106
