C₂₁H₂₅FO₄

Base Information

Chemical Name:C₂₁H₂₅FO₄
CAS No.:1181680-84-1
Molecular Formula:C₂₁H₂₅FO₄
Molecular Weight:360.426
Hs Code.:

C<sub>21</sub>H<sub>25</sub>FO<sub>4</sub>

Synonyms:

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of C₂₁H₂₅FO₄

Chemical Property:

Purity/Quality:

Safty Information:

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MSDS Files:

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Technology Process of C₂₁H₂₅FO₄

There total 12 articles about C₂₁H₂₅FO₄ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 10257-28-0
D-Galactose

: 1181680-84-1
C₂₁H₂₅FO₄

Guidance literature:: Multi-step reaction with 13 steps

1.1: pyridine / dmap / dichloromethane / 3.33 h / 35 °C / Reflux

2.1: triethylamine / dmap / dichloromethane

3.1: BAST / tetrahydrofuran / 2 h / 20 °C / Cooling with water

4.1: hydrogen bromide; acetic acid / 1 h / 20 °C

5.1: potassium carbonate / dichloromethane; N,N-dimethyl-formamide / 2 h / 20 °C

6.1: sodium methylate / methanol / 12 h / Reflux

7.1: sodium hydride / N,N-dimethyl-formamide; mineral oil / 2 h / 20 °C

8.1: N-Bromosuccinimide / acetone / 2 h / 20 °C

9.1: water / ethyl acetate

10.1: acetic anhydride / dimethyl sulfoxide / 20 °C

11.1: n-butyllithium / toluene; tetrahydrofuran / 0.17 h / -78 °C / Inert atmosphere

11.2: 0.5 h / -78 °C

12.1: boron trifluoride diethyl etherate; triethylsilane / acetonitrile / 0.5 h / -40 °C / Inert atmosphere

13.1: hydrogenchloride; hydrogen / palladium 10% on activated carbon / dichloromethane; methanol / 2 h / 4500.45 Torr

With pyridine; hydrogenchloride; triethylsilane; N-Bromosuccinimide; n-butyllithium; boron trifluoride diethyl etherate; water; hydrogen bromide; hydrogen; sodium methylate; acetic anhydride; sodium hydride; potassium carbonate; acetic acid; triethylamine; dmap; palladium 10% on activated carbon; In tetrahydrofuran; methanol; dichloromethane; dimethyl sulfoxide; ethyl acetate; N,N-dimethyl-formamide; acetone; toluene; acetonitrile; mineral oil;

Reference yield:

: 153527-47-0
1,2,3,6-tetra-O-trimethylacetyl-β-D-galactopyranose

: 1181680-84-1
C₂₁H₂₅FO₄

Guidance literature:: Multi-step reaction with 11 steps

1.1: BAST / tetrahydrofuran / 2 h / 20 °C / Cooling with water

2.1: hydrogen bromide; acetic acid / 1 h / 20 °C

3.1: potassium carbonate / dichloromethane; N,N-dimethyl-formamide / 2 h / 20 °C

4.1: sodium methylate / methanol / 12 h / Reflux

5.1: sodium hydride / N,N-dimethyl-formamide; mineral oil / 2 h / 20 °C

6.1: N-Bromosuccinimide / acetone / 2 h / 20 °C

7.1: water / ethyl acetate

8.1: acetic anhydride / dimethyl sulfoxide / 20 °C

9.1: n-butyllithium / toluene; tetrahydrofuran / 0.17 h / -78 °C / Inert atmosphere

9.2: 0.5 h / -78 °C

10.1: boron trifluoride diethyl etherate; triethylsilane / acetonitrile / 0.5 h / -40 °C / Inert atmosphere

11.1: hydrogenchloride; hydrogen / palladium 10% on activated carbon / dichloromethane; methanol / 2 h / 4500.45 Torr

With hydrogenchloride; triethylsilane; N-Bromosuccinimide; n-butyllithium; boron trifluoride diethyl etherate; water; hydrogen bromide; hydrogen; sodium methylate; acetic anhydride; sodium hydride; potassium carbonate; acetic acid; palladium 10% on activated carbon; In tetrahydrofuran; methanol; dichloromethane; dimethyl sulfoxide; ethyl acetate; N,N-dimethyl-formamide; acetone; toluene; acetonitrile; mineral oil;

Reference yield:

: (3R,4R,5R,6R)-3,4-bis(benzyloxy)-6-((benzyloxy)methyl)-5-fluorotetrahydro-2H-pyran-2-ol

: 1181680-84-1
C₂₁H₂₅FO₄

Guidance literature:: Multi-step reaction with 4 steps

1.1: acetic anhydride / dimethyl sulfoxide / 20 °C

2.1: n-butyllithium / toluene; tetrahydrofuran / 0.17 h / -78 °C / Inert atmosphere

2.2: 0.5 h / -78 °C

3.1: boron trifluoride diethyl etherate; triethylsilane / acetonitrile / 0.5 h / -40 °C / Inert atmosphere

4.1: hydrogenchloride; hydrogen / palladium 10% on activated carbon / dichloromethane; methanol / 2 h / 4500.45 Torr

With hydrogenchloride; triethylsilane; n-butyllithium; boron trifluoride diethyl etherate; hydrogen; acetic anhydride; palladium 10% on activated carbon; In tetrahydrofuran; methanol; dichloromethane; dimethyl sulfoxide; toluene; acetonitrile;