C₄₆H₄₆Cl₄N₄O₁₃

Base Information

Chemical Name:C₄₆H₄₆Cl₄N₄O₁₃
CAS No.:1398044-86-4
Molecular Formula:C₄₆H₄₆Cl₄N₄O₁₃
Molecular Weight:1004.7
Hs Code.:

C<sub>46</sub>H<sub>46</sub>Cl<sub>4</sub>N<sub>4</sub>O<sub>13</sub>

Synonyms:

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Chemical Property of C₄₆H₄₆Cl₄N₄O₁₃

Chemical Property:

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Technology Process of C₄₆H₄₆Cl₄N₄O₁₃

There total 4 articles about C₄₆H₄₆Cl₄N₄O₁₃ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: C₄₄H₄₆ClN₃O₁₃

: 545-06-2
trichloroacetonitrile

: 1398047-61-4
C₄₆H₄₆Cl₄N₄O₁₃

: 1398044-86-4
C₄₆H₄₆Cl₄N₄O₁₃

Guidance literature:: With sodium hydride; In dichloromethane; mineral oil; for 0.0833333h; Overall yield = 85 %; Overall yield = 2.84 g; Cooling with ice;
DOI:10.1002/chem.201204519

Reference yield:

: 1398044-75-1
4-methoxyphenyl 2-O-benzoyl-3-O-benzyl-6-O-chloroacetyl-β-D-glucopyranoside

: 1398047-61-4
C₄₆H₄₆Cl₄N₄O₁₃

: 1398044-86-4
C₄₆H₄₆Cl₄N₄O₁₃

Guidance literature:: Multi-step reaction with 3 steps

1: N-iodo-succinimide; silver trifluoromethanesulfonate / dichloromethane; toluene / 1 h / -15 - 20 °C / Inert atmosphere; Molecular sieve

2: ammonium cerium (IV) nitrate / water; acetonitrile / 20 °C / Inert atmosphere

3: sodium hydride / dichloromethane; mineral oil / 1 h / 20 °C / Inert atmosphere; Cooling

With N-iodo-succinimide; ammonium cerium (IV) nitrate; silver trifluoromethanesulfonate; sodium hydride; In dichloromethane; water; toluene; acetonitrile; mineral oil;
DOI:10.1039/c8ob02756k

Reference yield:

: C₂₉H₃₁N₃O₆S

: 1398047-61-4
C₄₆H₄₆Cl₄N₄O₁₃

: 1398044-86-4
C₄₆H₄₆Cl₄N₄O₁₃

Guidance literature:: Multi-step reaction with 3 steps

1: N-iodo-succinimide; silver trifluoromethanesulfonate / dichloromethane; toluene / 1 h / -15 - 20 °C / Inert atmosphere; Molecular sieve

2: ammonium cerium (IV) nitrate / water; acetonitrile / 20 °C / Inert atmosphere

3: sodium hydride / dichloromethane; mineral oil / 1 h / 20 °C / Inert atmosphere; Cooling

With N-iodo-succinimide; ammonium cerium (IV) nitrate; silver trifluoromethanesulfonate; sodium hydride; In dichloromethane; water; toluene; acetonitrile; mineral oil;
DOI:10.1039/c8ob02756k