4-methoxyphenyl 2-O-benzoyl-3-O-benzyl-6-O-chloroacetyl-β-D-glucopyranoside

Base Information

Chemical Name:4-methoxyphenyl 2-O-benzoyl-3-O-benzyl-6-O-chloroacetyl-β-D-glucopyranoside
CAS No.:1398044-75-1
Molecular Formula:C₂₉H₂₉ClO₉
Molecular Weight:556.997
Hs Code.:

Synonyms:4-methoxyphenyl 2-O-benzoyl-3-O-benzyl-6-O-chloroacetyl-β-D-glucopyranoside

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 4-methoxyphenyl 2-O-benzoyl-3-O-benzyl-6-O-chloroacetyl-β-D-glucopyranoside

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Technology Process of 4-methoxyphenyl 2-O-benzoyl-3-O-benzyl-6-O-chloroacetyl-β-D-glucopyranoside

There total 1 articles about 4-methoxyphenyl 2-O-benzoyl-3-O-benzyl-6-O-chloroacetyl-β-D-glucopyranoside which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 88.0%

: 79-04-9
chloroacetyl chloride

: 428865-77-4
4-methoxyphenyl 2-O-benzyol-3-O-benzyl-β-D-glucopyranoside

: 1398044-75-1
4-methoxyphenyl 2-O-benzoyl-3-O-benzyl-6-O-chloroacetyl-β-D-glucopyranoside

Guidance literature:: With pyridine; In dichloromethane; at -75 ℃; for 1h;
DOI:10.1002/chem.201204519

Reference yield: 79.0%

: 1398044-75-1
4-methoxyphenyl 2-O-benzoyl-3-O-benzyl-6-O-chloroacetyl-β-D-glucopyranoside

: C₂₉H₃₁N₃O₆S

: 1398044-77-3
4-methoxyphenyl 4-O-(6-O-acetyl-2-azido-3,4-di-O-benzyl-2-deoxy-α-D-glucopyranosyl)-2-O-benzoyl-3-O-benzyl-6-O-chloroacetyl-β-D-glucopyranoside

Guidance literature:: With N-iodo-succinimide; silver trifluoromethanesulfonate; In dichloromethane; toluene; at -15 - 20 ℃; for 1h; Inert atmosphere; Molecular sieve;
DOI:10.1039/c8ob02756k

Reference yield: 79.0%

: 1398044-65-9
methyl 2-azido-6-O-acetyl-3,4-di-O-benzyl-2-deoxy-1-thio-β-D-glucopyranoside

: 1398044-75-1
4-methoxyphenyl 2-O-benzoyl-3-O-benzyl-6-O-chloroacetyl-β-D-glucopyranoside

: 1398044-77-3
4-methoxyphenyl 4-O-(6-O-acetyl-2-azido-3,4-di-O-benzyl-2-deoxy-α-D-glucopyranosyl)-2-O-benzoyl-3-O-benzyl-6-O-chloroacetyl-β-D-glucopyranoside

Guidance literature:: methyl 2-azido-6-O-acetyl-3,4-di-O-benzyl-2-deoxy-1-thio-β-D-glucopyranoside; 4-methoxyphenyl 2-O-benzoyl-3-O-benzyl-6-O-chloroacetyl-β-D-glucopyranoside; In dichloromethane; toluene; at -15 ℃; for 0.166667h; Molecular sieve;

With N-iodo-succinimide; silver trifluoromethanesulfonate; In dichloromethane; toluene; at 20 ℃; for 1h; Molecular sieve;
DOI:10.1002/chem.201204519