C₆₁H₁₀₂N₂O₁₆S

Base Information

Chemical Name:C₆₁H₁₀₂N₂O₁₆S
CAS No.:1310452-86-8
Molecular Formula:C₆₁H₁₀₂N₂O₁₆S
Molecular Weight:1151.55
Hs Code.:

C<sub>61</sub>H<sub>102</sub>N<sub>2</sub>O<sub>16</sub>S

Synonyms:

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of C₆₁H₁₀₂N₂O₁₆S

Chemical Property:

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Technology Process of C₆₁H₁₀₂N₂O₁₆S

There total 14 articles about C₆₁H₁₀₂N₂O₁₆S which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 70.0%

: 108-30-5
succinic acid anhydride

: 1235550-15-8
C₅₇H₁₀₀N₂O₁₄S

: 1310452-86-8
C₆₁H₁₀₂N₂O₁₆S

: 1235550-18-1
C₆₁H₁₀₄N₂O₁₇S

Guidance literature:: With dmap; benzotriazol-1-ol; at 70 ℃; for 24h;
DOI:10.1016/j.bmcl.2011.03.056

Reference yield:

: 1235550-10-3
C₁₂H₁₈N₂O₅S

: 1310452-86-8
C₆₁H₁₀₂N₂O₁₆S

Guidance literature:: Multi-step reaction with 5 steps

1: tetra-(n-butyl)ammonium iodide; caesium carbonate / N,N-dimethyl-formamide / 8 h / 90 °C

2: cadmium(II) carbonate / benzene / 1.5 h / Reflux

3: 10% palladium on activated charcoal; ammonium formate / tetrahydrofuran; methanol / 0.5 h / 60 °C

4: dmap; triethylamine / dichloromethane / 36 h / 24 °C

5: 1,1'-carbonyldiimidazole

With dmap; cadmium(II) carbonate; 10% palladium on activated charcoal; ammonium formate; tetra-(n-butyl)ammonium iodide; caesium carbonate; triethylamine; 1,1'-carbonyldiimidazole; In tetrahydrofuran; methanol; dichloromethane; N,N-dimethyl-formamide; benzene;
DOI:10.1016/j.bmcl.2011.03.056

Reference yield:

: 1235550-11-4
C₄₃H₈₀N₂O₇S

: 1310452-86-8
C₆₁H₁₀₂N₂O₁₆S

Guidance literature:: Multi-step reaction with 4 steps

1: cadmium(II) carbonate / benzene / 1.5 h / Reflux

2: 10% palladium on activated charcoal; ammonium formate / tetrahydrofuran; methanol / 0.5 h / 60 °C

3: dmap; triethylamine / dichloromethane / 36 h / 24 °C

4: 1,1'-carbonyldiimidazole

With dmap; cadmium(II) carbonate; 10% palladium on activated charcoal; ammonium formate; triethylamine; 1,1'-carbonyldiimidazole; In tetrahydrofuran; methanol; dichloromethane; benzene;
DOI:10.1016/j.bmcl.2011.03.056