C₃₀H₃₆BrNO₂

Base Information

Chemical Name:C₃₀H₃₆BrNO₂
CAS No.:1565829-31-3
Molecular Formula:C₃₀H₃₆BrNO₂
Molecular Weight:522.525
Hs Code.:

C<sub>30</sub>H<sub>36</sub>BrNO<sub>2</sub>

Synonyms:

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of C₃₀H₃₆BrNO₂

Chemical Property:

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Technology Process of C₃₀H₃₆BrNO₂

There total 8 articles about C₃₀H₃₆BrNO₂ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 1565829-28-8
C₂₅H₂₆BrNO₂

: C₆H₉CuN^(1-)*Li⁽¹⁺⁾

: 1565829-31-3
C₃₀H₃₆BrNO₂

: 1565829-32-4
C₃₀H₃₆BrNO₂

Guidance literature:: C₂₅H₂₆BrNO₂; C₆H₉CuN^(1-)*Li⁽¹⁺⁾; With chloro-trimethyl-silane; In tetrahydrofuran; at -78 ℃; for 1h; Inert atmosphere;

With tetrabutyl ammonium fluoride; In tetrahydrofuran; Overall yield = 68 %; Overall yield = 39.2 mg; enantiospecific reaction; Inert atmosphere;
DOI:10.1021/ja501142e

Reference yield:

: 1565829-23-3
C₂₄H₂₆BrNO₂

: 1565829-31-3
C₃₀H₃₆BrNO₂

: 1565829-32-4
C₃₀H₃₆BrNO₂

Guidance literature:: Multi-step reaction with 2 steps

1.1: lithium hexamethyldisilazane / tetrahydrofuran / 2.5 h / -78 - 20 °C / Inert atmosphere

1.2: 0.25 h / 0 - 23 °C / Inert atmosphere

2.1: chloro-trimethyl-silane / tetrahydrofuran / 1 h / -78 °C / Inert atmosphere

2.2: Inert atmosphere

With chloro-trimethyl-silane; lithium hexamethyldisilazane; In tetrahydrofuran;
DOI:10.1021/ja501142e

Reference yield:

: 1565829-14-2
C₁₃H₇BrF₃NO₃S

: 1565829-31-3
C₃₀H₃₆BrNO₂

: 1565829-32-4
C₃₀H₃₆BrNO₂

Guidance literature:: Multi-step reaction with 6 steps

1.1: sodium hydride / tetrahydrofuran; mineral oil / 0.17 h / 0 °C / Inert atmosphere

1.2: 0.33 h / Inert atmosphere

2.1: 9-bora-bicyclo[3.3.1]nonane / tetrahydrofuran / 5 h / -78 - 23 °C / Inert atmosphere

2.2: 24 h / 65 °C / Inert atmosphere

3.1: tetrabutyl ammonium fluoride / tetrahydrofuran / 0.33 h / 23 °C / Inert atmosphere

4.1: 1-hydroxy-3H-benz[d][1,2]iodoxole-1,3-dione; 4-methylmorpholine N-oxide / dimethyl sulfoxide / 19 h / 45 °C / Inert atmosphere

5.1: lithium hexamethyldisilazane / tetrahydrofuran / 2.5 h / -78 - 20 °C / Inert atmosphere

5.2: 0.25 h / 0 - 23 °C / Inert atmosphere

6.1: chloro-trimethyl-silane / tetrahydrofuran / 1 h / -78 °C / Inert atmosphere

6.2: Inert atmosphere

With chloro-trimethyl-silane; tetrabutyl ammonium fluoride; sodium hydride; 4-methylmorpholine N-oxide; 9-bora-bicyclo[3.3.1]nonane; lithium hexamethyldisilazane; 1-hydroxy-3H-benz[d][1,2]iodoxole-1,3-dione; In tetrahydrofuran; dimethyl sulfoxide; mineral oil;
DOI:10.1021/ja501142e