Technology Process of C16H9ClIN5O
There total 11 articles about C16H9ClIN5O which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
Multi-step reaction with 7 steps
1: hydrogen bromide; acetic acid
2: potassium tert-butylate / N,N-dimethyl-formamide / -50 - 20 °C
3: sodium acetate / 20 °C
4: 1,8-diazabicyclo[5.4.0]undec-7-ene / 50 °C
5: trichlorophosphate
6: hydrazine
With
potassium tert-butylate; hydrogen bromide; sodium acetate; acetic acid; 1,8-diazabicyclo[5.4.0]undec-7-ene; hydrazine; trichlorophosphate;
In
N,N-dimethyl-formamide;
DOI:10.1016/j.bmcl.2011.09.016
- Guidance literature:
-
Multi-step reaction with 6 steps
1: potassium tert-butylate / N,N-dimethyl-formamide / -50 - 20 °C
2: sodium acetate / 20 °C
3: 1,8-diazabicyclo[5.4.0]undec-7-ene / 50 °C
4: trichlorophosphate
5: hydrazine
With
potassium tert-butylate; sodium acetate; 1,8-diazabicyclo[5.4.0]undec-7-ene; hydrazine; trichlorophosphate;
In
N,N-dimethyl-formamide;
DOI:10.1016/j.bmcl.2011.09.016
- Guidance literature:
-
Multi-step reaction with 6 steps
1: potassium tert-butylate / N,N-dimethyl-formamide / -50 - 20 °C
2: sodium acetate / 20 °C
3: 1,8-diazabicyclo[5.4.0]undec-7-ene / 50 °C
4: trichlorophosphate
5: hydrazine
With
potassium tert-butylate; sodium acetate; 1,8-diazabicyclo[5.4.0]undec-7-ene; hydrazine; trichlorophosphate;
In
N,N-dimethyl-formamide;
DOI:10.1016/j.bmcl.2011.09.016
