methyl 3,3,4,4,5,5-hexahydro-3-phenylbenzoazepin-1-one-4-carboxylate

Base Information

Chemical Name:methyl 3,3,4,4,5,5-hexahydro-3-phenylbenzoazepin-1-one-4-carboxylate
CAS No.:128080-54-6
Molecular Formula:C₁₈H₁₇NO₃
Molecular Weight:295.338
Hs Code.:

methyl 3,3,4,4,5,5-hexahydro-3-phenylbenzo<c>azepin-1-one-4-carboxylate

Synonyms:

Suppliers and Price of methyl 3,3,4,4,5,5-hexahydro-3-phenylbenzoazepin-1-one-4-carboxylate

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of methyl 3,3,4,4,5,5-hexahydro-3-phenylbenzoazepin-1-one-4-carboxylate

Chemical Property:

Purity/Quality:

Safty Information:

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Technology Process of methyl 3,3,4,4,5,5-hexahydro-3-phenylbenzoazepin-1-one-4-carboxylate

There total 4 articles about methyl 3,3,4,4,5,5-hexahydro-3-phenylbenzoazepin-1-one-4-carboxylate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 70.0%

: 127845-15-2,127845-22-1
(Z)-methyl 3-phenyl-4-hydroxyimino-1,2,3,4-tetrahydronaphthalene-2-carboxylate

: 128080-54-6
methyl 3,3,4,4,5,5-hexahydro-3-phenylbenzoazepin-1-one-4-carboxylate

Guidance literature:: With formic acid; acetic anhydride; tin(ll) chloride; at 50 - 60 ℃; for 4h;

Reference yield:

: 104958-17-0
diethyl 2-phenyl-1,2,3,4-tetrahydronapthalene-1-one-3,3-dicarboxylate

: 128080-54-6
methyl 3,3,4,4,5,5-hexahydro-3-phenylbenzoazepin-1-one-4-carboxylate

Guidance literature:: Multi-step reaction with 4 steps

1: 70 percent / KOH, water / ethane-1,2-diol; dioxane / 3 h / Heating

2: 98 percent / diethyl ether / 10 h / 20 °C

3: 78 percent / hydroxylamine hydrochloride, pyridine / 10 h / Heating

4: 70 percent / acetic anhydride, formic acid, stannous chloride / 4 h / 50 - 60 °C

With pyridine; potassium hydroxide; formic acid; hydroxylamine hydrochloride; water; acetic anhydride; tin(ll) chloride; In 1,4-dioxane; diethyl ether; ethylene glycol;

Reference yield:

: 128080-53-5
trans-(2R^*,3S^*)-3-phenyl-1,2,3,4-tetrahydronaphthalen-4-one-2-carboxylic acid

: 128080-54-6
methyl 3,3,4,4,5,5-hexahydro-3-phenylbenzoazepin-1-one-4-carboxylate

Guidance literature:: Multi-step reaction with 3 steps

1: 98 percent / diethyl ether / 10 h / 20 °C

2: 78 percent / hydroxylamine hydrochloride, pyridine / 10 h / Heating

3: 70 percent / acetic anhydride, formic acid, stannous chloride / 4 h / 50 - 60 °C

With pyridine; formic acid; hydroxylamine hydrochloride; acetic anhydride; tin(ll) chloride; In diethyl ether;