N-(α-phenylethyl)thiocrotonamide

Base Information

• Chemical Name: N-(α-phenylethyl)thiocrotonamide
• CAS No.: 139633-18-4
• Molecular Formula: C₁₂H₁₅NS
• Molecular Weight: 205.324

Synonyms:

Chemical Property of N-(α-phenylethyl)thiocrotonamide

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Technology Process of N-(α-phenylethyl)thiocrotonamide

There total 1 articles about N-(α-phenylethyl)thiocrotonamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

N-(α-phenylethyl)crotonamide (137160-70-4) → N-(α-phenylethyl)thiocrotonamide (139633-18-4)

Guidance literature:

With Lawessons reagent; In benzene; for 2h; Heating;

DOI:10.1021/jo00034a040

Reference yield: 70.0%

N-(α-phenylethyl)thiocrotonamide (139633-18-4) → N-(4-methyl-2-thietanylidene)-α-phenylethylamine (910618-91-6)

Guidance literature:

In benzene; Ambient temperature; Irradiation;

DOI:10.1021/jo00034a040

upstream raw materials:

N-(α-phenylethyl)crotonamide

Downstream raw materials:

N-(4-methyl-2-thietanylidene)-α-phenylethylamine

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