4,8-dihydroxyeudesmin

Base Information

Chemical Name:4,8-dihydroxyeudesmin
CAS No.:72536-34-6
Molecular Formula:C₂₂H₂₆O₈
Molecular Weight:418.444
Hs Code.:

Synonyms:

Suppliers and Price of 4,8-dihydroxyeudesmin

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 4,8-dihydroxyeudesmin

Chemical Property:

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Technology Process of 4,8-dihydroxyeudesmin

There total 8 articles about 4,8-dihydroxyeudesmin which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 96.0%

: 69854-19-9
2,6-bis-(3,4-dimethoxyphenyl)-3,7-dioxabicyclo<3.3.0>octane-4,8-dione

: 72536-34-6,111614-78-9
4,8-dihydroxyeudesmin

Guidance literature:: With diisobutylaluminum hydride; In tetrahydrofuran; hexane; at -68 ℃; for 3h;

Reference yield:

: 38209-42-6
threo-2,3-bis-(α-hydroxy-4-hydroxy-3-methoxybenzyl)butane-1,4-diol

: 72536-34-6,111614-78-9
4,8-dihydroxyeudesmin

Guidance literature:: Multi-step reaction with 6 steps

1: HCl / ethanol / high temperature vacuum distillation or heating with KHSO₄ at 200 deg C under vacuum

2: 66 percent / HCl(conc.) / 0.5 h / Heating

3: 15 mg / HCl / acetone / 1 h / Heating

4: 21 mg / chromium trioxide / pyridine / 4 h / Heating

5: 82 percent / diethyl ether / 24 h / Ambient temperature

6: 96 percent / di-isobutylaluminium hydride / tetrahydrofuran; hexane / 3 h / -68 °C

With chromium(VI) oxide; hydrogenchloride; diisobutylaluminum hydride; In tetrahydrofuran; pyridine; diethyl ether; ethanol; hexane; acetone;

Reference yield:

: 72536-33-5,92216-42-7,139239-90-0
4,8-dihydroxypinoresinol

: 72536-34-6,111614-78-9
4,8-dihydroxyeudesmin

Guidance literature:: Multi-step reaction with 5 steps

1: 66 percent / HCl(conc.) / 0.5 h / Heating

2: 15 mg / HCl / acetone / 1 h / Heating

3: 21 mg / chromium trioxide / pyridine / 4 h / Heating

4: 82 percent / diethyl ether / 24 h / Ambient temperature

5: 96 percent / di-isobutylaluminium hydride / tetrahydrofuran; hexane / 3 h / -68 °C

With chromium(VI) oxide; hydrogenchloride; diisobutylaluminum hydride; In tetrahydrofuran; pyridine; diethyl ether; hexane; acetone;