n-butylphenyl(3-hydroxypropoxy)borane

Base Information

Chemical Name:n-butylphenyl(3-hydroxypropoxy)borane
CAS No.:97782-85-9
Molecular Formula:C₁₃H₂₁BO₂
Molecular Weight:220.12
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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of n-butylphenyl(3-hydroxypropoxy)borane

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Technology Process of n-butylphenyl(3-hydroxypropoxy)borane

There total 1 articles about n-butylphenyl(3-hydroxypropoxy)borane which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 92.0%

: 30169-71-2
2-n-butyl-1,3,2-dioxaborinane

: 591-51-5
phenyllithium

: 97782-85-9
n-butylphenyl(3-hydroxypropoxy)borane

Guidance literature:: In diethyl ether; byproducts: LiCl; 1 equiv of PhLi slowly adding to a soln. of the boronic ester at -78°C, stirring for 3 h at the same temp., 1 equiv of anhydrous HCl in ether adding, warming to room temp., stirring for 15 min; product content detd. by (11)B NMR spectrum;
DOI:10.1021/om00129a019