2-BUTYL-1,3,2-DIOXABORINANE

Base Information

• Chemical Name: 2-BUTYL-1,3,2-DIOXABORINANE
• CAS No.: 30169-71-2
• Molecular Formula: C7H15 B O2
• Molecular Weight: 142.006
• Hs Code.: 2934999090
• Mol file: 30169-71-2.mol

Synonyms:1-Butaneboronicacid, cyclic trimethylene ester (7CI,8CI); 2-Butyl-1,3,2-dioxaborinane; NSC146255

Chemical Property of 2-BUTYL-1,3,2-DIOXABORINANE

Chemical Property:

• Vapor Pressure: 1.99mmHg at 25°C
• Boiling Point: 170°Cat760mmHg
• Flash Point: 58.9°C
• PSA: 18.46000
• Density: 0.88g/cm³
• LogP: 1.71160

Purity/Quality:

99%,98%, ^*data from raw suppliers

2-BUTYL-1,3,2-DIOXABORINANE 95.00% ^*data from reagent suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

Technology Process of 2-BUTYL-1,3,2-DIOXABORINANE

There total 6 articles about 2-BUTYL-1,3,2-DIOXABORINANE which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

1-butylene (106-98-9,9003-28-5) → 2-n-butyl-1,3,2-dioxaborinane (30169-71-2)

Guidance literature:

In tetrahydrofuran;

Reference yield:

1-butylene (106-98-9,9003-28-5) + O,O'-bis(2,6-2,6-dioxaborinan-1-yl)propane-1,3-diol (20905-35-5) → 2-n-butyl-1,3,2-dioxaborinane (30169-71-2)

Guidance literature:

Multistep reaction; (i) BH₃*THF, (ii) /BRN= 1913020/;

DOI:10.1021/ja00726a052

Reference yield:

n-butyllithium (109-72-8,29786-93-4) + 2-chloro-[1,3,2]dioxaborinane (1003-43-6) → 2-n-butyl-1,3,2-dioxaborinane (30169-71-2)

Guidance literature:

In diethyl ether;

DOI:10.1039/jr9620001428

upstream raw materials:

1-butylene

O,O'-bis(2,6-2,6-dioxaborinan-1-yl)propane-1,3-diol

n-butyllithium

2-(bis-phenylsulfanyl-methyl)-[1,3,2]dioxaborinane

Downstream raw materials:

pentan-1-ol

n-butylphenyl(3-hydroxypropoxy)borane