5'-C-benzyl-2'-hydroxy-3',4'-dimethoxydihydrochalcone

Base Information

Chemical Name:5'-C-benzyl-2'-hydroxy-3',4'-dimethoxydihydrochalcone
CAS No.:105485-62-9
Molecular Formula:C₂₄H₂₄O₄
Molecular Weight:376.452
Hs Code.:

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Chemical Property of 5'-C-benzyl-2'-hydroxy-3',4'-dimethoxydihydrochalcone

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Technology Process of 5'-C-benzyl-2'-hydroxy-3',4'-dimethoxydihydrochalcone

There total 13 articles about 5'-C-benzyl-2'-hydroxy-3',4'-dimethoxydihydrochalcone which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 100-39-0
benzyl bromide

: 105485-62-9
5'-C-benzyl-2'-hydroxy-3',4'-dimethoxydihydrochalcone

Guidance literature:: Multi-step reaction with 5 steps

1: 2.1 g / KOH / methanol / 24 h / Ambient temperature

2: 270 mg / K₂CO₃, KI / acetone / 1.5 h / Heating

3: 220 mg / KOH / ethanol; dimethylsulfoxide

4: 25 mg / H₂ / 10percent Pd-C / ethyl acetate / 760 Torr / Ambient temperature

5: K₂CO₃ / acetone

With potassium hydroxide; hydrogen; potassium carbonate; potassium iodide; palladium on activated charcoal; In methanol; ethanol; dimethyl sulfoxide; ethyl acetate; acetone;

Reference yield:

: 105485-58-3
5'-C-benzyl-2'-hydroxy-3',4'-dimethoxychalcone

: 105485-62-9
5'-C-benzyl-2'-hydroxy-3',4'-dimethoxydihydrochalcone

Guidance literature:: With hydrogen; palladium on activated charcoal; In ethyl acetate;

Reference yield:

: 528-21-2
2',3',4'-trihydroxyacetophenone

: 105485-62-9
5'-C-benzyl-2'-hydroxy-3',4'-dimethoxydihydrochalcone

Guidance literature:: Multi-step reaction with 4 steps

1: 3.8 g / BF₃*Et₂O / dioxane / 8 h / 60 - 70 °C

2: 150 mg / K₂CO₃ / acetone / 0.83 h / Heating

3: 80 mg / aq. KOH / methanol / 1) reflux, 20 min, 2) r.t., 48 h

4: 30 mg / H₂ / 10percent Pd-C / ethyl acetate

With potassium hydroxide; boron trifluoride diethyl etherate; hydrogen; potassium carbonate; palladium on activated charcoal; In 1,4-dioxane; methanol; ethyl acetate; acetone;