Technology Process of C37H52O4
There total 3 articles about C37H52O4 which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
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869788-74-9
(4aS,6aS,6bR,12aR)-benzyl 2,2,6a,6b,9,9,12a-heptamethyl-10-oxo-1,2,3,4,4a,5,6,6a,6b,7,8,8a,9,10,11,12,12a,12b,13,14b-icosahydropicene-4a-carboxylate
- Guidance literature:
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With
lithium carbonate; 3-chloro-benzenecarboperoxoic acid;
In
dichloromethane;
at 20 ℃;
for 8h;
DOI:10.1021/np100064m
- Guidance literature:
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Multi-step reaction with 3 steps
1: Jones reagent / dichloromethane; acetone / 0 °C
2: potassium carbonate / N,N-dimethyl-formamide / 20 °C
3: lithium carbonate; 3-chloro-benzenecarboperoxoic acid / dichloromethane / 8 h / 20 °C
With
Jones reagent; lithium carbonate; potassium carbonate; 3-chloro-benzenecarboperoxoic acid;
In
dichloromethane; N,N-dimethyl-formamide; acetone;
1: Jones oxidation / 3: Baeyer-Villiger oxidation;
DOI:10.1021/np100064m
- Guidance literature:
-
Multi-step reaction with 2 steps
1: potassium carbonate / N,N-dimethyl-formamide / 20 °C
2: lithium carbonate; 3-chloro-benzenecarboperoxoic acid / dichloromethane / 8 h / 20 °C
With
lithium carbonate; potassium carbonate; 3-chloro-benzenecarboperoxoic acid;
In
dichloromethane; N,N-dimethyl-formamide;
2: Baeyer-Villiger oxidation;
DOI:10.1021/np100064m
