(2E,6Z)-3,7-(7-methyl-⁽¹³⁾C)dimethylocta-2,6-dienyl benzyl ether

Base Information

• Chemical Name: (2E,6Z)-3,7-(7-methyl-⁽¹³⁾C)dimethylocta-2,6-dienyl benzyl ether
• CAS No.: 108526-68-7
• Molecular Formula: C₁₇H₂₄O
• Molecular Weight: 245.366

Synonyms:

Chemical Property of (2E,6Z)-3,7-(7-methyl-⁽¹³⁾C)dimethylocta-2,6-dienyl benzyl ether

Chemical Property:

Purity/Quality:

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Technology Process of (2E,6Z)-3,7-(7-methyl-⁽¹³⁾C)dimethylocta-2,6-dienyl benzyl ether

There total 4 articles about (2E,6Z)-3,7-(7-methyl-⁽¹³⁾C)dimethylocta-2,6-dienyl benzyl ether which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

C17(13)CH26O4S → (2E,6Z)-3,7-(7-methyl-(13)C)dimethylocta-2,6-dienyl benzyl ether (108526-68-7)

Guidance literature:

With lithium aluminium tetrahydride; In tetrahydrofuran; at 25 ℃; for 2h; Yield given;

DOI:10.1002/hlca.19860690822

Reference yield:

(E)-4-methyl-6-(phenylmethoxy)-4-hexenal (32989-52-9) → (2E,6Z)-3,7-(7-methyl-(13)C)dimethylocta-2,6-dienyl benzyl ether (108526-68-7)

Guidance literature:

Multi-step reaction with 4 steps

1: oxirane / benzene / 20 h / 25 °C / then 75 deg C, 2 h

2: 97.8 percent / diisobutylaluminium hydride / diethyl ether; toluene / 0.25 h / 0 °C

3: Et₃N / diethyl ether / 1 h / -10 °C

4: LiAlH₄ / tetrahydrofuran / 2 h / 25 °C

With oxirane; lithium aluminium tetrahydride; diisobutylaluminium hydride; triethylamine; In tetrahydrofuran; diethyl ether; toluene; benzene;

DOI:10.1002/hlca.19860690822

Reference yield:

(2Z,6E)-8-benzyloxy-2,6-(2-methyl-(13)C)dimethylocta-2,6-dienol → (2E,6Z)-3,7-(7-methyl-(13)C)dimethylocta-2,6-dienyl benzyl ether (108526-68-7)

Guidance literature:

Multi-step reaction with 2 steps

1: Et₃N / diethyl ether / 1 h / -10 °C

2: LiAlH₄ / tetrahydrofuran / 2 h / 25 °C

With lithium aluminium tetrahydride; triethylamine; In tetrahydrofuran; diethyl ether;

DOI:10.1002/hlca.19860690822

upstream raw materials:

(E)-4-methyl-6-(phenylmethoxy)-4-hexenal

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