(1Z)-1-Chloro-1,3-butadiene

Base Information

• Chemical Name: (1Z)-1-Chloro-1,3-butadiene
• CAS No.: 10033-99-5
• Molecular Formula: C4H5Cl
• Molecular Weight: 88.5367
• Hs Code.: 2903299090
• Mol file: 10033-99-5.mol

Synonyms:cis-1-chloro-1,3-butadiene;(Z)-1-chlorobuta-1,3-diene;(Z)-1-Chlor-1,3-butadien;(Z)-1-chloro-1,3-butadiene;1c-chloro-buta-1,3-diene;(Z)-1-Chlorobutadiene;

Chemical Property of (1Z)-1-Chloro-1,3-butadiene

Chemical Property:

• Boiling Point: 66.8-67 °C
• PSA: 0.00000
• Density: 0.9553 g/cm3
• LogP: 1.92490

Purity/Quality:

98%,99%, ^*data from raw suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

Technology Process of (1Z)-1-Chloro-1,3-butadiene

There total 2 articles about (1Z)-1-Chloro-1,3-butadiene which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

3-buten-1-yne (689-97-4) → (1Z)-1-chloro-1,3-butadiene (10033-99-5) + 4-chloro-1,2-butadiene (25790-55-0) + chloroprene (126-99-8,14523-89-8,9010-98-4)

Guidance literature:

With hydrogenchloride; for 7.5h;

DOI:10.1016/j.tet.2008.07.081

Reference yield:

3-buten-1-yne (689-97-4) → (1Z)-1-chloro-1,3-butadiene (10033-99-5) + 1-chloro-1E,3-butadiene (16503-25-6) + 4-chloro-1,2-butadiene (25790-55-0) + chloroprene (126-99-8,14523-89-8,9010-98-4)

Guidance literature:

With hydrogenchloride; at 79.84 ℃; Activation energy;

DOI:10.1016/j.tet.2008.07.081

Reference yield:

1-Heptyne (628-71-7) + (1Z)-1-chloro-1,3-butadiene (10033-99-5) → 1,3-undecadien-5-yne (166432-52-6)

Guidance literature:

With piperidine; copper(l) iodide; bis(benzonitrile)palladium(II) dichloride; Yield given. Multistep reaction; 1.) RT, 15 min, 2.) RT, 30 min;

DOI:10.1080/00397919408019052

upstream raw materials:

3-buten-1-yne

Downstream raw materials:

1,3-undecadien-5-yne

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