N,N'''-<6<(4-phenyl-2-thiazolyl)sulfonyl>-2,4-quinazolinediyl>bis

Base Information

Chemical Name:N,N'''-<6<(4-phenyl-2-thiazolyl)sulfonyl>-2,4-quinazolinediyl>bis
CAS No.:74396-43-3
Molecular Formula:C₂₃H₂₃N₇O₂S₂
Molecular Weight:493.613
Hs Code.:

N,N'''-<6<(4-phenyl-2-thiazolyl)sulfonyl>-2,4-quinazolinediyl>bis<N,N-dimethylformamidine>

Synonyms:

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Chemical Property of N,N'''-<6<(4-phenyl-2-thiazolyl)sulfonyl>-2,4-quinazolinediyl>bis

Chemical Property:

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Technology Process of N,N'''-<6<(4-phenyl-2-thiazolyl)sulfonyl>-2,4-quinazolinediyl>bis

There total 6 articles about N,N'''-<6<(4-phenyl-2-thiazolyl)sulfonyl>-2,4-quinazolinediyl>bis which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 78.0%

: 74396-41-1
2,4-diamino-6-<(4-phenyl-2-thiazolyl)sulfonyl>quinazoline

: 4637-24-5
N,N-dimethyl-formamide dimethyl acetal

: 74396-43-3
N,N'''-<6<(4-phenyl-2-thiazolyl)sulfonyl>-2,4-quinazolinediyl>bis

Guidance literature:: In N,N-dimethyl-formamide; for 4h; Ambient temperature;
DOI:10.1002/jhet.5570170127

Reference yield:

: 2103-88-0
2-Mercapto-4-phenylthiazole

: 74396-43-3
N,N'''-<6<(4-phenyl-2-thiazolyl)sulfonyl>-2,4-quinazolinediyl>bis

Guidance literature:: Multi-step reaction with 5 steps

1: 40 percent / K₂CO₃ / acetone / 20 h / Ambient temperature

2: 66 percent / SnCl₂*2H₂O, conc. HCl / acetic acid / 18 h / Ambient temperature

3: 48 percent / various solvent(s) / 0.33 h / 160 °C

4: 63 percent / 30percent H₂O₂, acetic acid / 48 h / Ambient temperature

5: 78 percent / dimethylformamide / 4 h / Ambient temperature

With hydrogenchloride; dihydrogen peroxide; potassium carbonate; acetic acid; tin(ll) chloride; In acetic acid; N,N-dimethyl-formamide; acetone;
DOI:10.1002/jhet.5570170127

Reference yield:

: 34662-31-2
3-chloro-6-nitrobenzonitrile

: 74396-43-3
N,N'''-<6<(4-phenyl-2-thiazolyl)sulfonyl>-2,4-quinazolinediyl>bis

Guidance literature:: Multi-step reaction with 5 steps

1: 40 percent / K₂CO₃ / acetone / 20 h / Ambient temperature

2: 66 percent / SnCl₂*2H₂O, conc. HCl / acetic acid / 18 h / Ambient temperature

3: 48 percent / various solvent(s) / 0.33 h / 160 °C

4: 63 percent / 30percent H₂O₂, acetic acid / 48 h / Ambient temperature

5: 78 percent / dimethylformamide / 4 h / Ambient temperature

With hydrogenchloride; dihydrogen peroxide; potassium carbonate; acetic acid; tin(ll) chloride; In acetic acid; N,N-dimethyl-formamide; acetone;
DOI:10.1002/jhet.5570170127