Technology Process of 4,17-dibenzoyl-1,7,14,20-tetrakis(p-tolylsulfonyl)-1,4,7,14,17,20-hexaazacyclohexacosane
There total 5 articles about 4,17-dibenzoyl-1,7,14,20-tetrakis(p-tolylsulfonyl)-1,4,7,14,17,20-hexaazacyclohexacosane which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
Multi-step reaction with 4 steps
1: 77 percent / acetonitrile / Heating
2: 80 percent / triethylamine / benzene / temp. below 50 deg C, overnight
3: 95 percent / C2H5ONa / ethanol
4: 17 percent / dimethylformamide / 2 h / 95 °C
With
sodium ethanolate; triethylamine;
In
ethanol; N,N-dimethyl-formamide; acetonitrile; benzene;
DOI:10.1021/jo00342a006
- Guidance literature:
-
Multi-step reaction with 5 steps
1: 94 percent / 20percent aq. KOH / benzene / 0.5 h
2: 77 percent / acetonitrile / Heating
3: 80 percent / triethylamine / benzene / temp. below 50 deg C, overnight
4: 95 percent / C2H5ONa / ethanol
5: 17 percent / dimethylformamide / 2 h / 95 °C
With
potassium hydroxide; sodium ethanolate; triethylamine;
In
ethanol; N,N-dimethyl-formamide; acetonitrile; benzene;
DOI:10.1021/jo00342a006
- Guidance literature:
-
Multi-step reaction with 3 steps
1: 80 percent / triethylamine / benzene / temp. below 50 deg C, overnight
2: 95 percent / C2H5ONa / ethanol
3: 17 percent / dimethylformamide / 2 h / 95 °C
With
sodium ethanolate; triethylamine;
In
ethanol; N,N-dimethyl-formamide; benzene;
DOI:10.1021/jo00342a006
