C₂₄H₃₄N₄O₄

Base Information

• Chemical Name: C₂₄H₃₄N₄O₄
• CAS No.: 1333956-90-3
• Molecular Formula: C₂₄H₃₄N₄O₄
• Molecular Weight: 442.558
• Mol file: 1333956-90-3.mol

Synonyms:

Chemical Property of C₂₄H₃₄N₄O₄

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of C₂₄H₃₄N₄O₄

There total 4 articles about C₂₄H₃₄N₄O₄ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 60.0%

C38H46N4O4 (1333956-79-8) → C24H34N4O4 (1333956-90-3)

Guidance literature:

With 5%-palladium/activated carbon; water; ammonium formate; In methanol; for 5h; Reflux;

DOI:10.3762/bjoc.7.131

Reference yield:

1,6-Hexanediamine (124-09-4) → C24H34N4O4 (1333956-90-3)

Guidance literature:

Multi-step reaction with 4 steps

1: 5 h / Reflux

2: triethylamine; trichlorophosphate / dichloromethane / 0 °C

3: phenylphosphinic acid / methanol / 48 h / 20 °C

4: 5%-palladium/activated carbon; water; ammonium formate / methanol / 5 h / Reflux

With 5%-palladium/activated carbon; phenylphosphinic acid; water; ammonium formate; triethylamine; trichlorophosphate; In methanol; dichloromethane; 3: Ugi condensation;

DOI:10.3762/bjoc.7.131

Reference yield:

hexanediyldiformamide (35161-65-0) → C24H34N4O4 (1333956-90-3)

Guidance literature:

Multi-step reaction with 3 steps

1: triethylamine; trichlorophosphate / dichloromethane / 0 °C

2: phenylphosphinic acid / methanol / 48 h / 20 °C

3: 5%-palladium/activated carbon; water; ammonium formate / methanol / 5 h / Reflux

With 5%-palladium/activated carbon; phenylphosphinic acid; water; ammonium formate; triethylamine; trichlorophosphate; In methanol; dichloromethane; 2: Ugi condensation;

DOI:10.3762/bjoc.7.131

upstream raw materials:

1,6-Hexanediamine

C₃₈H₄₆N₄O₄

hexanediyldiformamide

1,6-di-isocyanohexane