C₅₃H₄₆O₁₅

Base Information

Chemical Name:C₅₃H₄₆O₁₅
CAS No.:847237-50-7
Molecular Formula:C₅₃H₄₆O₁₅
Molecular Weight:922.939
Hs Code.:

C<sub>53</sub>H<sub>46</sub>O<sub>15</sub>

Synonyms:

Suppliers and Price of C₅₃H₄₆O₁₅

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of C₅₃H₄₆O₁₅

Chemical Property:

Purity/Quality:

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Technology Process of C₅₃H₄₆O₁₅

There total 7 articles about C₅₃H₄₆O₁₅ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: C₆₀H₅₀O₁₇S

: 847237-50-7
C₅₃H₄₆O₁₅

Guidance literature:: With 2,2'-azobis(isobutyronitrile); tri-n-butyl-tin hydride; In benzene; at 80 ℃; for 1h;
DOI:10.1016/j.carres.2004.11.017

Reference yield:

: 34361-44-9
phenyl 2,3,4,6-tetra-O-acetyl-β-D-galactopyranosyl-(1→4)-2,3,6-tri-O-acetyl-α-D-glucopyranoside

: 847237-50-7
C₅₃H₄₆O₁₅

Guidance literature:: Multi-step reaction with 6 steps

1: 9.8 g / NaOMe / methanol / 20 °C

2: 3.0 g / H₂SO₄ / dimethylformamide; acetone / 1 h / Heating

3: 5.86 g / pyridine / 3 h / 20 °C

4: 89 percent / acetic acid; H₂O / 1 h / 95 °C

5: 4-(N,N-dimethylamino)pyridine / CH₂Cl₂ / 4 h / 20 °C

6: 0.30 g / tributyltin hydride; azoisobutyronitrile / benzene / 1 h / 80 °C

With dmap; 2,2'-azobis(isobutyronitrile); sulfuric acid; tri-n-butyl-tin hydride; sodium methylate; In pyridine; methanol; dichloromethane; water; acetic acid; N,N-dimethyl-formamide; acetone; benzene;
DOI:10.1016/j.carres.2004.11.017

Reference yield:

: 3616-19-1,5328-50-7,5346-90-7,6291-42-5,6920-00-9,20764-63-0,20880-60-8,20880-65-3,22352-19-8,23973-20-8,32447-69-1,34213-32-6,52554-32-2,53956-64-2,56907-29-0,56994-12-8,56994-13-9,57128-38-8,67650-36-6,68036-17-9,68036-19-1,78215-50-6,78215-51-7,79549-48-7,80446-82-8,85249-04-3,93221-83-1,93779-27-2,111407-83-1,111407-84-2,111407-85-3,120328-65-6,123809-59-6,132341-46-9,132341-47-0,132341-49-2,145307-94-4
1',2',3',6',2,3,4,6-octa-O-acetyl-β-D-lactose

: 847237-50-7
C₅₃H₄₆O₁₅

Guidance literature:: Multi-step reaction with 7 steps

1: 83 percent / molecular sieves 4 Angstroem; boron trifluoride etherate / CH₂Cl₂

2: 9.8 g / NaOMe / methanol / 20 °C

3: 3.0 g / H₂SO₄ / dimethylformamide; acetone / 1 h / Heating

4: 5.86 g / pyridine / 3 h / 20 °C

5: 89 percent / acetic acid; H₂O / 1 h / 95 °C

6: 4-(N,N-dimethylamino)pyridine / CH₂Cl₂ / 4 h / 20 °C

7: 0.30 g / tributyltin hydride; azoisobutyronitrile / benzene / 1 h / 80 °C

With dmap; 2,2'-azobis(isobutyronitrile); 4 A molecular sieve; sulfuric acid; boron trifluoride diethyl etherate; tri-n-butyl-tin hydride; sodium methylate; In pyridine; methanol; dichloromethane; water; acetic acid; N,N-dimethyl-formamide; acetone; benzene;
DOI:10.1016/j.carres.2004.11.017