5,5'-methylenebis(8-hydroxyquinoline)

Base Information

Chemical Name:5,5'-methylenebis(8-hydroxyquinoline)
CAS No.:2536-71-2
Molecular Formula:C₁₉H₁₄N₂O₂
Molecular Weight:302.332
Hs Code.:
Mol file:2536-71-2.mol

Synonyms:

Suppliers and Price of 5,5'-methylenebis(8-hydroxyquinoline)

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 2 raw suppliers

Chemical Property of 5,5'-methylenebis(8-hydroxyquinoline)

Chemical Property:

Purity/Quality:: 99% ^*data from raw suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Technology Process of 5,5'-methylenebis(8-hydroxyquinoline)

There total 6 articles about 5,5'-methylenebis(8-hydroxyquinoline) which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 52.0%

: 148-24-3,24804-14-6
8-quinolinol

: 50-00-0,30525-89-4,61233-19-0
formaldehyd

: 2536-71-2
5,5'-methylenebis(8-hydroxyquinoline)

Guidance literature:: With sulfuric acid; at 0 ℃; for 3h; Product distribution; other temperatures;

Reference yield:

: 23186-90-5
bis-(3-amino-4-methoxy-phenyl)-methane

: 56-81-5,25618-55-7,64333-26-2,8013-25-0
glycerol

: 2536-71-2
5,5'-methylenebis(8-hydroxyquinoline)

Guidance literature:: With arsenic(V) oxide; sulfuric acid; at 150 - 155 ℃; Erhitzen des Reaktionsprodukts mit wss. HBr;
DOI:10.1002/ardp.19582911004

Reference yield:

: 148-24-3,24804-14-6
8-quinolinol

: 2536-71-2
5,5'-methylenebis(8-hydroxyquinoline)

Guidance literature:: Multi-step reaction with 2 steps

1: water; hydrochloric acid; hydrogen chloride / und Behandeln des Reaktionsprodukts mit wss.Ammoniak oder wss.Natriumhydrogencarbonat-Loesung

2: acetic acid; concentrated H₂SO₄

With hydrogenchloride; sulfuric acid; water; acetic acid;
DOI:10.1002/ardp.19582911004