2-Amino-4,5-dimethoxybenzene-1-thiol

Base Information

Chemical Name:2-Amino-4,5-dimethoxybenzene-1-thiol
CAS No.:100601-30-7
Molecular Formula:C8H11NO2S
Molecular Weight:185.247
Hs Code.:
European Community (EC) Number:845-092-0
Nikkaji Number:J1.880.065I
Mol file:100601-30-7.mol

Synonyms:100601-30-7;2-amino-4,5-dimethoxybenzene-1-thiol;2-Amino-4,5-dimethoxybenzenethiol;SCHEMBL5112479;2-amino-4,5-dimethoxybenzene-thiol;AKOS014385957;EN300-341934;F8883-8726

Suppliers and Price of 2-Amino-4,5-dimethoxybenzene-1-thiol

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 2 raw suppliers

Chemical Property of 2-Amino-4,5-dimethoxybenzene-1-thiol

Chemical Property:

XLogP3:1.3
Hydrogen Bond Donor Count:2
Hydrogen Bond Acceptor Count:4
Rotatable Bond Count:2
Exact Mass:185.05104977
Heavy Atom Count:12
Complexity:145

Purity/Quality:: 99% ^*data from raw suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Canonical SMILES:COC1=C(C=C(C(=C1)N)S)OC

Technology Process of 2-Amino-4,5-dimethoxybenzene-1-thiol

There total 5 articles about 2-Amino-4,5-dimethoxybenzene-1-thiol which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 113037-07-3
bis(4,5-dimethoxyanilin-2-yl)disulfide

: 100601-30-7
2-amino-4,5-dimethoxy-thiophenol

Guidance literature:: With diothiothreitol; In N,N-dimethyl-formamide;
DOI:10.1002/anie.201004087

Reference yield:

: 6315-89-5
3,4-dimethoxyaniline

: 100601-30-7
2-amino-4,5-dimethoxy-thiophenol

Guidance literature:: Multi-step reaction with 3 steps

1.1: bromine; acetic acid / 0.5 h / 10 °C

1.2: 19 h / 10 °C

2.1: potassium hydroxide / water; ethylene glycol / 24 h / 140 °C

3.1: 1,4-dithio-D,L-threitol / N,N-dimethyl-formamide / 0.5 h / 20 °C

With 1,4-dithio-D,L-threitol; bromine; acetic acid; potassium hydroxide; In water; ethylene glycol; N,N-dimethyl-formamide;
DOI:10.1002/ejoc.201100818