Benzenediazonium, 3-chloro-, chloride

Base Information

• Chemical Name: Benzenediazonium, 3-chloro-, chloride
• CAS No.: 100-77-6
• Molecular Formula: C6H4ClN2.Cl
• Molecular Weight: 175.017
• DSSTox Substance ID: DTXSID10438153
• Mol file: 100-77-6.mol

Synonyms:Benzenediazonium, 3-chloro-, chloride;100-77-6;Benzenediazonium, 3-chloro-, chloride (1:1);FAST ORANGE GC SALT;3-chlorobenzenediazonium Chloride;AZOIC DIAZO COMPONENT 2;SCHEMBL5485232;m-chlorobenzenediazonium chloride;3-chlorobenzenediazonium;chloride;DTXSID10438153;RLNNKLNZXOUFDY-UHFFFAOYSA-M;Benzenediazonium, m-chloro-, chloride

Chemical Property of Benzenediazonium, 3-chloro-, chloride

Chemical Property:

• Hydrogen Bond Donor Count: 0
• Hydrogen Bond Acceptor Count: 2
• Rotatable Bond Count: 0
• Exact Mass: 173.9751535
• Heavy Atom Count: 10
• Complexity: 137

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

• Canonical SMILES: C1=CC(=CC(=C1)Cl)[N+]#N.[Cl-]

Technology Process of Benzenediazonium, 3-chloro-, chloride

There total 7 articles about Benzenediazonium, 3-chloro-, chloride which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 83.0%

C12H10ClN3O → 3-chlorobenzenediazonium chloride (100-77-6)

Guidance literature:

With oxalyl dichloride; In toluene; for 0.166667h; Ambient temperature;

DOI:10.1039/a605013a

Reference yield:

3-chloro-aniline (108-42-9) → 3-chlorobenzenediazonium chloride (100-77-6)

Guidance literature:

With sodium nitrite; In hydrogenchloride; water; at 25 ℃; Rate constant;

Reference yield:

3-chloroaniline hydrochloride (141-85-5) → 3-chlorobenzenediazonium chloride (100-77-6)

Guidance literature:

With tert.-butylnitrite; In acetonitrile; at 20 ℃; for 0.166667h;

DOI:10.1039/c5ob00245a

upstream raw materials:

3-chloro-aniline

C₁₄H₁₁ClN₄S

C₁₄H₁₁ClN₄S

isopentyl nitrite

Downstream raw materials:

1,3-Dichlorobenzene

3-phenyl-isoxazole-4,5-dione 4-[(3-chloro-phenyl)-hydrazone]

5-(3-chloro-phenylsulfanyl)-3-phenyl-3H-[1,3,4]thiadiazole-2-thione

2-[(3-Chloro-phenyl)-hydrazono]-1-(4,6-dimethoxy-benzofuran-5-yl)-butane-1,3-dione

Refernces

• 1、 Baumann, Marcus,Rodriguez Garcia, Antonio M.,Baxendale, Ian R.. "Flow synthesis of ethyl isocyanoacetate enabling the telescoped synthesis of 1,2,4-triazoles and pyrrolo-[1,2-c]pyrimidines". . p. 4231 - 4239. Retrieved 2015/04/14.
• 2、 -. "TRIAZOLE COMPOUNDS AND THEIR USE AS METABOTROPIC GLUTAMATE RECEPTOR ANTAGONISTS". Page/Page column 45-46. . Retrieved 2010/02/13.