1,1'-(But-1-ene-4,4-diyldisulfonyl)dibenzene

Base Information

Chemical Name:1,1'-(But-1-ene-4,4-diyldisulfonyl)dibenzene
CAS No.:100780-24-3
Molecular Formula:C16H16O4S2
Molecular Weight:336.433
Hs Code.:
DSSTox Substance ID:DTXSID50545991
Wikidata:Q82423666
Mol file:100780-24-3.mol

Synonyms:100780-24-3;1,1'-(But-1-ene-4,4-diyldisulfonyl)dibenzene;DTXSID50545991

Suppliers and Price of 1,1'-(But-1-ene-4,4-diyldisulfonyl)dibenzene

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

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Chemical Property of 1,1'-(But-1-ene-4,4-diyldisulfonyl)dibenzene

Chemical Property:

XLogP3:3.4
Hydrogen Bond Donor Count:0
Hydrogen Bond Acceptor Count:4
Rotatable Bond Count:6
Exact Mass:336.04900133
Heavy Atom Count:22
Complexity:506

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Canonical SMILES:C=CCC(S(=O)(=O)C1=CC=CC=C1)S(=O)(=O)C2=CC=CC=C2

Technology Process of 1,1'-(But-1-ene-4,4-diyldisulfonyl)dibenzene

There total 2 articles about 1,1'-(But-1-ene-4,4-diyldisulfonyl)dibenzene which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 94.0%

: 3406-02-8
bis(phenylsulfonyl)methane

: 106-95-6
allyl bromide

: 100780-24-3
1,1-bis(phenylsulfonyl)-3-butene

Guidance literature:: bis(phenylsulfonyl)methane; With sodium hydride; In N,N-dimethyl-formamide; mineral oil; at 0 ℃; for 0.5h; Inert atmosphere;

allyl bromide; In N,N-dimethyl-formamide; mineral oil; at 20 ℃; for 4h; Inert atmosphere;
DOI:10.1021/acs.joc.6b01799

Reference yield:

: 556-56-9
allyl iodid

: 3406-02-8
bis(phenylsulfonyl)methane

: 100780-24-3
1,1-bis(phenylsulfonyl)-3-butene

Guidance literature:: With sodium hydride; Yield given. Multistep reaction; 1.) THF, 0 deg C, 15 min, 2.) THF, reflux, 12 h;
DOI:10.1021/ja00132a005

Reference yield: 100.0%

: 136863-23-5
3-[2-(hydroxymethyl)phenyl]propan-1-ol

: 100780-24-3
1,1-bis(phenylsulfonyl)-3-butene

: 3-{o-[2,2-bis(phenylsulfonyl)-4-penten-1-yl]phenyl}-1-propanol

Guidance literature:: With tributylphosphine; diamide; triethylamine; In benzene; at 0 - 20 ℃; for 23h; Inert atmosphere;
DOI:10.1021/acs.joc.6b01799