O-methyl P,P-diphenylphosphinite borane

Base Information

Chemical Name:O-methyl P,P-diphenylphosphinite borane
CAS No.:34327-50-9
Molecular Formula:C₁₃H₁₆BOP
Molecular Weight:230.054
Hs Code.:

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Chemical Property of O-methyl P,P-diphenylphosphinite borane

Chemical Property:

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Technology Process of O-methyl P,P-diphenylphosphinite borane

There total 2 articles about O-methyl P,P-diphenylphosphinite borane which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 23308-76-1
C₁₄H₁₆O₂P⁽¹⁺⁾*CF₃O₃S^(1-)

: 34327-50-9
O-methyl P,P-diphenylphosphinite borane

Guidance literature:: With lithium borohydride; In tetrahydrofuran; at -78 ℃; chemoselective reaction; Inert atmosphere; Schlenk technique;
DOI:10.1039/c5cc06389b

Reference yield:

: 1706-90-7
methyl diphenylphosphinate

: 34327-50-9
O-methyl P,P-diphenylphosphinite borane

Guidance literature:: Multi-step reaction with 2 steps

1: 1,1,2,2-tetrachloroethylene / 16 h / 75 °C / Inert atmosphere; Schlenk technique

2: lithium borohydride / tetrahydrofuran / -78 °C / Inert atmosphere; Schlenk technique

With lithium borohydride; In tetrahydrofuran; 1,1,2,2-tetrachloroethylene;
DOI:10.1039/c5cc06389b

Reference yield:

: (Cp*)Mo(CO)3Me

: 34327-50-9
O-methyl P,P-diphenylphosphinite borane

: [(C₅(CH₃)5)Mo(CO)3(BH₂P(OCH₃)(C₆H₅)2)]

Guidance literature:: In hexane; byproducts: CH4; Irradiation (UV/VIS); (N2); Schlenk technique; mixt. of B compd. and Mo complex in hexane was irradiated at 0°C; NMR monitoring; not isolated;
DOI:10.1021/om0603159