{η5-(1-phenylborole)}tris(triethylphosphane)rhodium-bis{η5-(1-phenylborole)} rhodate

Base Information

Chemical Name:{η5-(1-phenylborole)}tris(triethylphosphane)rhodium-bis{η5-(1-phenylborole)} rhodate
CAS No.:118227-86-4
Molecular Formula:C₂₀H₁₈B₂Rh*C₂₈H₅₄BP₃Rh
Molecular Weight:980.265
Hs Code.:

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of {η5-(1-phenylborole)}tris(triethylphosphane)rhodium-bis{η5-(1-phenylborole)} rhodate

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Technology Process of {η5-(1-phenylborole)}tris(triethylphosphane)rhodium-bis{η5-(1-phenylborole)} rhodate

There total 1 articles about {η5-(1-phenylborole)}tris(triethylphosphane)rhodium-bis{η5-(1-phenylborole)} rhodate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 86.0%

: 87883-14-5
μ-(η5-C4H4B(C6H5)){Rh(η5-C4H4B(C6H5))}2

: 554-70-1
triethylphosphine

: 118227-86-4
{η5-(1-phenylborole)}tris(triethylphosphane)rhodium-bis{η5-(1-phenylborole)} rhodate

Guidance literature:: In tetrahydrofuran; (N2); to soln. of Rh complex was added excess of PEt3, after color had changed from orange to yellow volatiles were removed in vac.; residue was stirred with diethyl ether, filtered, washed with ether and recrystd. from actone/ether; elem. anal.;

Reference yield:

: 118227-86-4
{η5-(1-phenylborole)}tris(triethylphosphane)rhodium-bis{η5-(1-phenylborole)} rhodate

: 594-09-2
trimethylphosphane

: {(C₄H₄BC₆H₅)RhP(C₂H₅)3(P(CH₃)3)2}⁽¹⁺⁾*{Rh(C₄H₄BC₆H₅)2}^(1-)={(C₄H₄BC₆H₅)RhP(C₂H₅)3(P(CH₃)3)2}{Rh(C₄H₄BC₆H₅)2}

: 118227-90-0
{(C₄H₄BC₆H₅)Rh(P(C₂H₅)3)2P(CH₃)3}⁽¹⁺⁾*{Rh(C₄H₄BC₆H₅)2}^(1-)={(C₄H₄BC₆H₅)Rh(P(C₂H₅)3)2P(CH₃)3}{Rh(C₄H₄BC₆H₅)2}

: 110795-50-1
(η5-1-phenylborole)tris(trimethylphosphine)rhodium {bis(η5-1-phenylborole)rhodate}

Guidance literature:: In dichloromethane-d2; (N2); to soln. of Rh complex was added PMe3 and mixt. was kept at room temp. for 2 h; not isolated, identified by (31)P-NMR; Kinetics;