2,2′,5,5′-tetramethyl-4,4′-azodiacetanilide

Base Information

Chemical Name:2,2′,5,5′-tetramethyl-4,4′-azodiacetanilide
CAS No.:106423-99-8
Molecular Formula:C₂₀H₂₄N₄O₂
Molecular Weight:352.436
Hs Code.:

Synonyms:

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Chemical Property of 2,2′,5,5′-tetramethyl-4,4′-azodiacetanilide

Chemical Property:

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Technology Process of 2,2′,5,5′-tetramethyl-4,4′-azodiacetanilide

There total 4 articles about 2,2′,5,5′-tetramethyl-4,4′-azodiacetanilide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 33.0%

: 23410-20-0
2,5-dimethyl-4-aminoacetanilide

: 106423-99-8
2,2′,5,5′-tetramethyl-4,4′-azodiacetanilide

Guidance literature:: With sodium peroxoborate tetrahydrate; boric acid; acetic acid; at 45 - 50 ℃; for 5.5h;
DOI:10.1021/ic502487x

Reference yield:

: 6954-69-4
N-(2,5-dimethyl-4-nitrophenyl)acetamide

: 106423-99-8
2,2′,5,5′-tetramethyl-4,4′-azodiacetanilide

Guidance literature:: Multi-step reaction with 2 steps

1.1: iron(III) chloride hexahydrate; pyrographite / ethanol / 0.25 h / Reflux

1.2: 16 h / Reflux

2.1: acetic acid; boric acid; sodium peroxoborate tetrahydrate / 5.5 h / 45 - 50 °C

With sodium peroxoborate tetrahydrate; iron(III) chloride hexahydrate; boric acid; pyrographite; acetic acid; In ethanol;
DOI:10.1021/ic502487x

Reference yield:

: 95-78-3
2,5-Dimethylaniline

: 106423-99-8
2,2′,5,5′-tetramethyl-4,4′-azodiacetanilide

Guidance literature:: Multi-step reaction with 4 steps

1.1: sulfuric acid; nitric acid / -10 °C

2.1: sodium carbonate / acetone / 18 h / Reflux

3.1: iron(III) chloride hexahydrate; pyrographite / ethanol / 0.25 h / Reflux

3.2: 16 h / Reflux

4.1: acetic acid; boric acid; sodium peroxoborate tetrahydrate / 5.5 h / 45 - 50 °C

With sodium peroxoborate tetrahydrate; iron(III) chloride hexahydrate; sulfuric acid; nitric acid; boric acid; sodium carbonate; pyrographite; acetic acid; In ethanol; acetone;
DOI:10.1021/ic502487x