t-butyl 6-O-[6'-O-[6''-O-(benzyl)-2'',3''-dideoxy-β-D-threo-hex-2''-enopyranosyl]-2',3'-dideoxy-β-D-threo-hex-2'-enopyranosyl]-2,3-dideoxy-β-D-threo-hex-2-enopyranoside

Base Information

• Chemical Name: t-butyl 6-O-[6'-O-[6''-O-(benzyl)-2'',3''-dideoxy-β-D-threo-hex-2''-enopyranosyl]-2',3'-dideoxy-β-D-threo-hex-2'-enopyranosyl]-2,3-dideoxy-β-D-threo-hex-2-enopyranoside
• CAS No.: 1033614-50-4
• Molecular Formula: C₂₉H₄₀O₁₀
• Molecular Weight: 548.631

Synonyms:

Chemical Property of t-butyl 6-O-[6'-O-[6''-O-(benzyl)-2'',3''-dideoxy-β-D-threo-hex-2''-enopyranosyl]-2',3'-dideoxy-β-D-threo-hex-2'-enopyranosyl]-2,3-dideoxy-β-D-threo-hex-2-enopyranoside

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
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MSDS Files:

Useful:

Technology Process of t-butyl 6-O-[6'-O-[6''-O-(benzyl)-2'',3''-dideoxy-β-D-threo-hex-2''-enopyranosyl]-2',3'-dideoxy-β-D-threo-hex-2'-enopyranosyl]-2,3-dideoxy-β-D-threo-hex-2-enopyranoside

There total 3 articles about t-butyl 6-O-[6'-O-[6''-O-(benzyl)-2'',3''-dideoxy-β-D-threo-hex-2''-enopyranosyl]-2',3'-dideoxy-β-D-threo-hex-2'-enopyranosyl]-2,3-dideoxy-β-D-threo-hex-2-enopyranoside which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

t-butyl 6-O-[6'-O-[6''-O-(benzyl)-4''-O-acetyl-2'',3''-dideoxy-β-D-threo-hex-2''-enopyranosyl]-4'-O-acetyl-2',3'-dideoxy-β-D-threo-hex-2'-enopyranosyl]-2,3-dideoxy-β-D-threo-hex-2-enopyranoside (1033614-46-8) → t-butyl 6-O-[6'-O-[6''-O-(benzyl)-2'',3''-dideoxy-β-D-threo-hex-2''-enopyranosyl]-2',3'-dideoxy-β-D-threo-hex-2'-enopyranosyl]-2,3-dideoxy-β-D-threo-hex-2-enopyranoside (1033614-50-4)

Guidance literature:

With methanol; sodium methylate; at 20 ℃; for 18h; Inert atmosphere;

DOI:10.1021/ol800793f

Reference yield:

t-butyl 6-O-[6'-O-[6''-O-(benzyl)-4''-O-acetyl-2'',3''-dideoxy-β-D-threo-hex-2''-enopyranosyl]-4'-O-acetyl-2',3'-dideoxy-β-D-threo-hex-2'-enopyranosyl]-4-O-acetyl-2,3-dideoxy-β-D-threo-hex-2-enopyranoside (1033614-48-0) → t-butyl 6-O-[6'-O-[6''-O-(benzyl)-2'',3''-dideoxy-β-D-threo-hex-2''-enopyranosyl]-2',3'-dideoxy-β-D-threo-hex-2'-enopyranosyl]-2,3-dideoxy-β-D-threo-hex-2-enopyranoside (1033614-50-4)

Guidance literature:

With methanol; sodium methylate; at 20 ℃; for 18h; Inert atmosphere;

DOI:10.1021/ol800793f

Reference yield:

6-O-[6'-O-[6''-O-(benzyl)-2'',3''-dideoxy-β-D-threo-hex-2''-enopyranosyl]-2',3'-dideoxy-β-D-threo-hex-2'-enopyranosyl]-4-O-mesyl-D-glucal (1033614-56-0) + tert-butyl alcohol (75-65-0) → t-butyl 6-O-[6'-O-[6''-O-(benzyl)-2'',3''-dideoxy-β-D-threo-hex-2''-enopyranosyl]-2',3'-dideoxy-β-D-threo-hex-2'-enopyranosyl]-2,3-dideoxy-β-D-threo-hex-2-enopyranoside (1033614-50-4)

Guidance literature:

With potassium tert-butylate; at 20 ℃; for 18h; Inert atmosphere;

DOI:10.1021/ol800793f

upstream raw materials:

t-butyl 6-O-[6'-O-[6''-O-(benzyl)-4''-O-acetyl-2'',3''-dideoxy-β-D-threo-hex-2''-enopyranosyl]-4'-O-acetyl-2',3'-dideoxy-β-D-threo-hex-2'-enopyranosyl]-2,3-dideoxy-β-D-threo-hex-2-enopyranoside

t-butyl 6-O-[6'-O-[6''-O-(benzyl)-4''-O-acetyl-2'',3''-dideoxy-β-D-threo-hex-2''-enopyranosyl]-4'-O-acetyl-2',3'-dideoxy-β-D-threo-hex-2'-enopyranosyl]-4-O-acetyl-2,3-dideoxy-β-D-threo-hex-2-enopyranoside

6-O-[6'-O-[6''-O-(benzyl)-2'',3''-dideoxy-β-D-threo-hex-2''-enopyranosyl]-2',3'-dideoxy-β-D-threo-hex-2'-enopyranosyl]-4-O-mesyl-D-glucal

tert-butyl alcohol

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