Na-bis(borole)cobaltate

Base Information

Chemical Name:Na-bis(borole)cobaltate
CAS No.:111800-81-8
Molecular Formula:C₂₀H₁₈B₂Co*Na
Molecular Weight:361.968
Hs Code.:

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Chemical Property of Na-bis(borole)cobaltate

Chemical Property:

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Technology Process of Na-bis(borole)cobaltate

There total 2 articles about Na-bis(borole)cobaltate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 82.0%

: 111800-75-0
μ-{η5-(1-phenylborole)}-bis{η5-(1-phenylborole)cobalt}

: {C5H5Co(η5-C4H4BPh)}

: 111800-81-8
Na-bis(borole)cobaltate

Guidance literature:: With cyclopentadienyl sodium; In tetrahydrofuran; refluxed for 3 d under N2; evapd., residue was treated with CH2Cl2 and water, org. phase extd. with water, satd. aq. NaCl was added to the water exts., ppt. was filtered off, dried, dissolved in CH2Cl2, filtered, evapn. gave Na-salt; CpCo(C4H4BPh) was isolated from org. phase;
DOI:10.1016/0022-328X(87)80343-1

Reference yield:

: 111800-75-0
μ-{η5-(1-phenylborole)}-bis{η5-(1-phenylborole)cobalt}

: 111800-81-8
Na-bis(borole)cobaltate

Guidance literature:: With sodium amalgam; In tetrahydrofuran; byproducts: cobalt;
DOI:10.1016/0022-328X(87)80343-1

Reference yield: 88.0%

: caesium nitrate

: 111800-81-8
Na-bis(borole)cobaltate

: 111800-82-9
caesium-{bis{η5-(1-phenylborole)}cobaltate}

Guidance literature:: In water; aq. soln. of CsNO3 was added to a soln. of Co-complex in water under N2; ppt. was filtered off, dried, recrystd. from acetone-Et2O; elem. anal.;
DOI:10.1016/0022-328X(87)80343-1