zirconocene isobutyl pentafluorophenoxide

Base Information

Chemical Name:zirconocene isobutyl pentafluorophenoxide
CAS No.:1187043-25-9
Molecular Formula:C₂₀H₁₉F₅OZr
Molecular Weight:461.586
Hs Code.:

Synonyms:

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of zirconocene isobutyl pentafluorophenoxide

Chemical Property:

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Technology Process of zirconocene isobutyl pentafluorophenoxide

There total 3 articles about zirconocene isobutyl pentafluorophenoxide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 35.0%

: 90491-53-5
zirconocene bis(pentafluorophenoxide)

: 5674-02-2
2-methylpropylmagnesium chloride

: 1187043-25-9
zirconocene isobutyl pentafluorophenoxide

Guidance literature:: In diethyl ether; under inert atmosphere; Zr complex dissolved in Et2O; cooled to -78°C; Et2O soln. of i-BuMgCl added dropwise; stirred at -78°C for1 h; warmed to room temp.; stirred for 1.5 h; volatiles removed under vac.; dried for 15 min; hexane added; stirred; evapd.; extd. with hexane; filtered; evapd. to dryness;
DOI:10.1021/om8008734

Reference yield:

: 1187043-19-1
zirconocene tert-butyl pentafluorophenoxide

: 1187043-25-9
zirconocene isobutyl pentafluorophenoxide

Guidance literature:: In benzene-d6; under inert atmosphere; soln. of Zr complex in benzene-d6 stored at 70°C for 3 h; monitored by (1)H NMR spectra; Kinetics;
DOI:10.1021/om8008734

Reference yield:

: 13269-52-8
trans-3-Hexene

: 1187043-19-1
zirconocene tert-butyl pentafluorophenoxide

: 1187043-25-9
zirconocene isobutyl pentafluorophenoxide

: 1187043-33-9
zirconocene n-hexyl pentafluorophenoxide

Guidance literature:: In benzene-d6; under inert atmosphere; in sealed NMR tube; Zr complex and trans-3-hexene in benzene-d6 heated at 70°C for 3 h; volatiles removed in vac.; taken up in benzene-d6; detd. by NMR spectra;
DOI:10.1021/om8008734