benzyl O-(2-azido-3,4,6-tri-O-benzyl-2-deoxy-β-D-mannopyranosyl)-(1->6)-2,3,4-tri-O-benzyl-β-D-glucopyranoside

Base Information

Chemical Name:benzyl O-(2-azido-3,4,6-tri-O-benzyl-2-deoxy-β-D-mannopyranosyl)-(1->6)-2,3,4-tri-O-benzyl-β-D-glucopyranoside
CAS No.:106837-24-5
Molecular Formula:C₆₁H₆₃N₃O₁₀
Molecular Weight:998.185
Hs Code.:

Synonyms:

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Chemical Property of benzyl O-(2-azido-3,4,6-tri-O-benzyl-2-deoxy-β-D-mannopyranosyl)-(1->6)-2,3,4-tri-O-benzyl-β-D-glucopyranoside

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Technology Process of benzyl O-(2-azido-3,4,6-tri-O-benzyl-2-deoxy-β-D-mannopyranosyl)-(1->6)-2,3,4-tri-O-benzyl-β-D-glucopyranoside

There total 7 articles about benzyl O-(2-azido-3,4,6-tri-O-benzyl-2-deoxy-β-D-mannopyranosyl)-(1->6)-2,3,4-tri-O-benzyl-β-D-glucopyranoside which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 95451-96-0
Allyl-2-azido-3,4,6-tri-O-benzyl-2-desoxy-α-D-mannopyranosid

: 106837-24-5
benzyl O-(2-azido-3,4,6-tri-O-benzyl-2-deoxy-β-D-mannopyranosyl)-(1->6)-2,3,4-tri-O-benzyl-β-D-glucopyranoside

Guidance literature:: Multi-step reaction with 3 steps

1: 95 percent / (1,5-cyclooctadiene)bis(methyldiphenylphosphine)iridium-hexafluorophosphate / tetrahydrofuran / 2 h / Ambient temperature

3: 81 percent / silver silicate, molecular sieves / toluene / 18 h / -30 °C

With molecular sieve; silver silicate; (1,5-cyclooctadiene)[bis(methyldiphenylphosphine)]iridium(I) hexafluorophosphate; In tetrahydrofuran; toluene;

Reference yield:

: 100-39-0
benzyl bromide

: 106837-24-5
benzyl O-(2-azido-3,4,6-tri-O-benzyl-2-deoxy-β-D-mannopyranosyl)-(1->6)-2,3,4-tri-O-benzyl-β-D-glucopyranoside

Guidance literature:: Multi-step reaction with 3 steps

1: 535 mg / NaH / dimethylformamide / 1 h / Ambient temperature

2: 67 percent Turnov_. / 30 percent H₂SO₄ / acetic acid / 4 h / 95 °C

3: p-NO₂C₆H₄SO₂Cl, AgOTf, Et₃N / CH₂Cl₂ / 1) -60 deg C to 0 deg C, 2) overnight

With sulfuric acid; silver trifluoromethanesulfonate; sodium hydride; triethylamine; 4-Nitrobenzenesulfonyl chloride; In dichloromethane; acetic acid; N,N-dimethyl-formamide;
DOI:10.1246/bcsj.72.765

Reference yield:

: 223545-38-8
methyl 2-azido-2-deoxy-α-D-mannopyranoside

: 106837-24-5
benzyl O-(2-azido-3,4,6-tri-O-benzyl-2-deoxy-β-D-mannopyranosyl)-(1->6)-2,3,4-tri-O-benzyl-β-D-glucopyranoside

Guidance literature:: Multi-step reaction with 3 steps

1: 535 mg / NaH / dimethylformamide / 1 h / Ambient temperature

2: 67 percent Turnov_. / 30 percent H₂SO₄ / acetic acid / 4 h / 95 °C

3: p-NO₂C₆H₄SO₂Cl, AgOTf, Et₃N / CH₂Cl₂ / 1) -60 deg C to 0 deg C, 2) overnight

With sulfuric acid; silver trifluoromethanesulfonate; sodium hydride; triethylamine; 4-Nitrobenzenesulfonyl chloride; In dichloromethane; acetic acid; N,N-dimethyl-formamide;
DOI:10.1246/bcsj.72.765