2-Phenyl-1H-benz<1,4>oxazepin

Base Information

Chemical Name:2-Phenyl-1H-benz<1,4>oxazepin
CAS No.:130627-19-9
Molecular Formula:C₁₅H₁₁NO₂
Molecular Weight:237.258
Hs Code.:

Synonyms:

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 2-Phenyl-1H-benz<1,4>oxazepin

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Technology Process of 2-Phenyl-1H-benz<1,4>oxazepin

There total 6 articles about 2-Phenyl-1H-benz<1,4>oxazepin which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 77.0%

: 130627-10-0
anthranilic acid phenacylester

: 130627-19-9
2-Phenyl-1H-benz<1,4>oxazepin

Guidance literature:: With Polyphosphorsaeure; at 100 ℃; for 2h;

Reference yield:

: 118-92-3,159201-01-1,50816-84-7,80206-34-4,104809-47-4
anthranilic acid

: 130627-19-9
2-Phenyl-1H-benz<1,4>oxazepin

Guidance literature:: Multi-step reaction with 2 steps

1: 81 percent / potassium carbonate / acetone / 5 h / Heating

2: 59 percent / phosphoryl chloride / benzene / 2 h / Heating; different phenacyl anthranilate derivatives

With potassium carbonate; trichlorophosphate; In acetone; benzene;
DOI:10.1016/0040-4020(95)00880-H

Reference yield:

: 70-11-1
α-bromoacetophenone

: 130627-19-9
2-Phenyl-1H-benz<1,4>oxazepin

Guidance literature:: Multi-step reaction with 2 steps

1: 81 percent / potassium carbonate / acetone / 5 h / Heating

2: 59 percent / phosphoryl chloride / benzene / 2 h / Heating; different phenacyl anthranilate derivatives

With potassium carbonate; trichlorophosphate; In acetone; benzene;
DOI:10.1016/0040-4020(95)00880-H