N-<3-<<4-<(3-Aminopropyl)amino>butyl>amino>propyl>-4-toluolsulfonamid Hydrochlorid

Base Information

Chemical Name:N-<3-<<4-<(3-Aminopropyl)amino>butyl>amino>propyl>-4-toluolsulfonamid Hydrochlorid
CAS No.:134935-58-3
Molecular Formula:C₁₇H₃₂N₄O₂S*ClH
Molecular Weight:392.994
Hs Code.:

Synonyms:

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Chemical Property of N-<3-<<4-<(3-Aminopropyl)amino>butyl>amino>propyl>-4-toluolsulfonamid Hydrochlorid

Chemical Property:

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Technology Process of N-<3-<<4-<(3-Aminopropyl)amino>butyl>amino>propyl>-4-toluolsulfonamid Hydrochlorid

There total 6 articles about N-<3-<<4-<(3-Aminopropyl)amino>butyl>amino>propyl>-4-toluolsulfonamid Hydrochlorid which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 107199-54-2
3-<(4-Hydroxybutyl)amino>propannitril

: 134935-58-3
N-<3-<<4-<(3-Aminopropyl)amino>butyl>amino>propyl>-4-toluolsulfonamid Hydrochlorid

Guidance literature:: Multi-step reaction with 5 steps

1: H₂, conc. HCl / PtO₂ / ethanol / 20 h / 22 °C / 2585.7 Torr

2: 95 percent / Na₂CO₃ / dioxane; H₂O / 1 h

3: 26 percent / oxalyl chloride / dimethylsulfoxide; CH₂Cl₂ / 0.5 h / -50 °C

4: 17 mg / 3-Angstroem molecular sieves, NaBH₄ / ethanol / 0.33 h / 0 °C

5: 10 mg / HCl / diethyl ether

With hydrogenchloride; sodium tetrahydroborate; oxalyl dichloride; 3 A molecular sieve; hydrogen; sodium carbonate; platinum(IV) oxide; In 1,4-dioxane; diethyl ether; ethanol; dichloromethane; water; dimethyl sulfoxide;
DOI:10.1002/hlca.19910740322

Reference yield:

: 134935-57-2
O,O'-Di(tert-butyl)-N,N'-(propan-1,3-diyl)-N-<4-<<3-(tosylamino)propyl>amino>butyl>bis

: 134935-58-3
N-<3-<<4-<(3-Aminopropyl)amino>butyl>amino>propyl>-4-toluolsulfonamid Hydrochlorid

Guidance literature:: With hydrogenchloride; In diethyl ether;
DOI:10.1002/hlca.19910740322

Reference yield:

: 38353-77-4
N-(N³-p-toluenesulfonyl)-3-aminopropylphthalimide

: 134935-58-3
N-<3-<<4-<(3-Aminopropyl)amino>butyl>amino>propyl>-4-toluolsulfonamid Hydrochlorid

Guidance literature:: Multi-step reaction with 3 steps

1: 70 percent / N₂H₄*H₂O / ethanol / 1 h / Heating

2: 17 mg / 3-Angstroem molecular sieves, NaBH₄ / ethanol / 0.33 h / 0 °C

3: 10 mg / HCl / diethyl ether

With hydrogenchloride; sodium tetrahydroborate; 3 A molecular sieve; hydrazine hydrate; In diethyl ether; ethanol;
DOI:10.1002/hlca.19910740322