fac-(cis-1,5-bis((diphenylphosphino)-methyl)-3-oxabicyclo{3.3.0}octane-P,P')tricarbonyl(1-methyl-4-phospha-3,5,8-trioxabicyclo{2.2.2}octane-P)tungsten

Base Information

Chemical Name:fac-(cis-1,5-bis((diphenylphosphino)-methyl)-3-oxabicyclo{3.3.0}octane-P,P')tricarbonyl(1-methyl-4-phospha-3,5,8-trioxabicyclo{2.2.2}octane-P)tungsten
CAS No.:139344-46-0
Molecular Formula:C₄₁H₄₃O₇P₃W
Molecular Weight:924.56
Hs Code.:

fac-(cis-1,5-bis((diphenylphosphino)-methyl)-3-oxabicyclo{3.3.0}octane-P,P')tricarbonyl(1-methyl-4-phospha-3,5,8-trioxabicyclo{2.2.2}octane-P)tungsten

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Chemical Property of fac-(cis-1,5-bis((diphenylphosphino)-methyl)-3-oxabicyclo{3.3.0}octane-P,P')tricarbonyl(1-methyl-4-phospha-3,5,8-trioxabicyclo{2.2.2}octane-P)tungsten

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Technology Process of fac-(cis-1,5-bis((diphenylphosphino)-methyl)-3-oxabicyclo{3.3.0}octane-P,P')tricarbonyl(1-methyl-4-phospha-3,5,8-trioxabicyclo{2.2.2}octane-P)tungsten

There total 1 articles about fac-(cis-1,5-bis((diphenylphosphino)-methyl)-3-oxabicyclo{3.3.0}octane-P,P')tricarbonyl(1-methyl-4-phospha-3,5,8-trioxabicyclo{2.2.2}octane-P)tungsten which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 67.0%

: 134848-45-6
fac-(cis-1,5-bis((diphenylphosphino)-(methyl))-3-oxabicyclo{3.3.0}octane-P,P',O)W(CO)3

: 1449-91-8
4-methyl-2,6,7-trioxa-1-phosphabicyclo-[2,2,2]-octane

: 139344-45-9
fac-(cis-1,5-bis((diphenylphosphino)-methyl)-3-oxabicyclo{3.3.0}octane-P,P')tricarbonyl(1-methyl-4-phospha-3,5,8-trioxabicyclo{2.2.2}octane-P)tungsten

: 139344-46-0
fac-(cis-1,5-bis((diphenylphosphino)-methyl)-3-oxabicyclo{3.3.0}octane-P,P')tricarbonyl(1-methyl-4-phospha-3,5,8-trioxabicyclo{2.2.2}octane-P)tungsten

Guidance literature:: In dichloromethane; addn. of the ligand (soln.) to a soln. of the complex, stirring for 20 min, loss in color; filtration, washing (pentane), drying (vacuo), isomeres not separated, elem. anal.;
DOI:10.1021/om00040a022