1,4-bis(4-methoxyphenyl)-2,3-diphenyl-1,4-diaza-1,3-butadiene*ZrCl₄

Base Information

• Chemical Name: 1,4-bis(4-methoxyphenyl)-2,3-diphenyl-1,4-diaza-1,3-butadiene*ZrCl₄
• CAS No.: 143744-93-8
• Molecular Formula: C₂₈H₂₄Cl₄N₂O₂Zr
• Molecular Weight: 653.547

Synonyms:

Chemical Property of 1,4-bis(4-methoxyphenyl)-2,3-diphenyl-1,4-diaza-1,3-butadiene*ZrCl₄

Chemical Property:

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Technology Process of 1,4-bis(4-methoxyphenyl)-2,3-diphenyl-1,4-diaza-1,3-butadiene*ZrCl₄

There total 1 articles about 1,4-bis(4-methoxyphenyl)-2,3-diphenyl-1,4-diaza-1,3-butadiene*ZrCl₄ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 68.0%

zirconium chloride-tetrahydrofuran + 1,4-bis-(4-methoxyphenyl)-2,3-diphenyl-1,4-diaza-1,3-butadiene (32349-49-8) → 1,4-bis(4-methoxyphenyl)-2,3-diphenyl-1,4-diaza-1,3-butadiene*ZrCl4 (143744-93-8)

Guidance literature:

In dichloromethane; exclusion of air and moisture, under Ar; dissolving the Zr-compd. in CH2Cl2 and addn. of the diazadiene under stirring, heating the soln. for 2 h to moderate boiling and then cooling slowly; filtering off the pptd. crystals and drying; elem. anal.;

upstream raw materials:

1,4-bis-(4-methoxyphenyl)-2,3-diphenyl-1,4-diaza-1,3-butadiene

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