C₂₅H₃₄N₂O₄

Base Information

Chemical Name:C₂₅H₃₄N₂O₄
CAS No.:1338085-83-8
Molecular Formula:C₂₅H₃₄N₂O₄
Molecular Weight:426.556
Hs Code.:

C<sub>25</sub>H<sub>34</sub>N<sub>2</sub>O<sub>4</sub>

Synonyms:

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of C₂₅H₃₄N₂O₄

Chemical Property:

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Technology Process of C₂₅H₃₄N₂O₄

There total 2 articles about C₂₅H₃₄N₂O₄ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 34.0%

: 1338085-79-2
C₂₀H₂₀Br₂O₄

: 109-55-7
1-amino-3-(dimethylamino)propane

: 1338085-83-8
C₂₅H₃₄N₂O₄

: 1338085-81-6
C₂₅H₃₂N₂O₄

Guidance literature:: With {2-[2-(azanidyl-κN)ethyl]phenyl-κC¹}{[2',6'-bis(propan-2-yloxy)biphenyl-2-yl](dicyclohexyl)-λ⁵-phosphanyl}chloropalladium; potassium carbonate; XPhos; In tert-butyl alcohol; at 140 ℃; for 1.5h; Microwave irradiation;
DOI:10.1002/chem.201100885

Reference yield:

: 83536-13-4
bis(4-ethoxycarbonylphenyl)acetylene

: 1338085-83-8
C₂₅H₃₄N₂O₄

: 1338085-81-6
C₂₅H₃₂N₂O₄

Guidance literature:: Multi-step reaction with 3 steps

1: palladium on activated charcoal; hydrogen / dichloromethane; ethyl acetate / 20 °C

2: 1,3-dibromo-5,5-dimethylimidazolidine-2,4-dione; trifluorormethanesulfonic acid / dichloromethane / 2 h / 20 °C

3: {2-[2-(azanidyl-κN)ethyl]phenyl-κC¹}{[2',6'-bis(propan-2-yloxy)biphenyl-2-yl](dicyclohexyl)-λ⁵-phosphanyl}chloropalladium; potassium carbonate; XPhos / tert-butyl alcohol / 1.5 h / 140 °C / Microwave irradiation

With 1,3-dibromo-5,5-dimethylimidazolidine-2,4-dione; trifluorormethanesulfonic acid; palladium on activated charcoal; {2-[2-(azanidyl-κN)ethyl]phenyl-κC¹}{[2',6'-bis(propan-2-yloxy)biphenyl-2-yl](dicyclohexyl)-λ⁵-phosphanyl}chloropalladium; hydrogen; potassium carbonate; XPhos; In dichloromethane; ethyl acetate; tert-butyl alcohol;
DOI:10.1002/chem.201100885