[(N(2,6-diisopropylphenyl)CH)2]GeH₂

Base Information

• Chemical Name: [(N(2,6-diisopropylphenyl)CH)2]GeH₂
• CAS No.: 1241380-40-4
• Molecular Formula: C₂₆H₃₈GeN₂
• Molecular Weight: 451.191

Synonyms:

Chemical Property of [(N(2,6-diisopropylphenyl)CH)2]GeH₂

Chemical Property:

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Technology Process of [(N(2,6-diisopropylphenyl)CH)2]GeH₂

There total 1 articles about [(N(2,6-diisopropylphenyl)CH)2]GeH₂ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 84.0%

trimethylamine alane (16842-00-5,855944-65-9) + [(N(2,6-diisopropylphenyl)CH)2]GeCl2 → [(N(2,6-diisopropylphenyl)CH)2]GeH2 (1241380-40-4)

Guidance literature:

In toluene; byproducts: trimethylamine, AlH2Cl; (N2); addn. of a soln. of Al compd. in toluene to a soln. of Ge complex in toluene at -10°C, warming to room temp., stirring for 1 h; evapn. in vac., extn. with n-hexane, evapn.;

DOI:10.1039/c002395g

Reference yield: 72.0%

[(N(2,6-diisopropylphenyl)CH)2]GeH2 (1241380-40-4) → 1,3-bis(2,6-diisopropylphenyl)diazagermol-2-ylidene (880761-37-5)

Guidance literature:

With B(C₆F₅)3; 1,3-di-tert-butylimidazol-2-ylidene; In toluene; byproducts: 1,3-di-tert-butylimidazolium HB(C6F5)3; (N2); dropwise addn. of a soln. of carbene in toluene to a stirred soln.of Ge complex in toluene at room temp., dropwise addn. of a soln. of bo ron compd. in toluene, react. for 30 min; evapn. in vac., extn. with n-hexane;

DOI:10.1039/c002395g

upstream raw materials:

trimethylamine alane

Downstream raw materials:

1,3-bis(2,6-diisopropylphenyl)diazagermol-2-ylidene

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